N~3~-methyl-beta-alaninamide(SALTDATA: HCl)

Base Information

• Chemical Name: N~3~-methyl-beta-alaninamide(SALTDATA: HCl)
• CAS No.: 4874-17-3
• Molecular Formula: C4H10N2O
• Molecular Weight: 102.135
• Hs Code.: 2924199090
• Mol file: 4874-17-3.mol

Synonyms:N~3~-methyl-beta-alaninamide(SALTDATA: HCl);3-(Methylamino)propionamide, N-Methyl-beta-alanamide;3-(MethylaMino)propionaMide;3-(Methylamino)propionamide 95%

Chemical Property of N~3~-methyl-beta-alaninamide(SALTDATA: HCl)

Chemical Property:

• Refractive Index: n20/D1.485
• Boiling Point: 274.5±23.0 °C(Predicted)
• PKA: 16.43±0.40(Predicted)
• Flash Point: >110℃
• PSA: 56.11000
• Density: 1.052 g/mL at 25 °C
• LogP: 0.62180

Purity/Quality:

98%,99%, ^*data from raw suppliers

3-(Methylamino)propanamide ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N~3~-methyl-beta-alaninamide(SALTDATA: HCl)

There total 3 articles about N~3~-methyl-beta-alaninamide(SALTDATA: HCl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N-(2-cyanoethyl)-N-methylamine (693-05-0) → N-methyl-β-alaninamide (4874-17-3)

Guidance literature:

With potassium hydroxide; In tert-butyl alcohol; at 90 ℃; for 1h;

DOI:10.1016/S0968-0896(00)00279-0

Reference yield: 51.0%

3-chloropropionamide (5875-24-1) + methylamine (74-89-5) → N-methyl-β-alaninamide (4874-17-3)

Guidance literature:

In water; at 0 - 5 ℃; for 5h;

DOI:10.1021/jm00021a013

Reference yield:

→ N-methyl-β-alaninamide (4874-17-3)

Guidance literature:

2-Methylamino-1-cyan-ethan, konz. H2SO4;

upstream raw materials:

3-chloropropionamide

methylamine

N-(2-cyanoethyl)-N-methylamine

Downstream raw materials:

3-(methyl((3-(5-phenyl-4-(trifluoromethyl)isoxazol-3-yl)-4,5-dihydronaphtho[1,2-c]isoxazol-7-yl)methyl)amino)propanamide

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