4-BroMo-2-iodo-benzoic acid Methyl ester

Base Information

• Chemical Name: 4-BroMo-2-iodo-benzoic acid Methyl ester
• CAS No.: 1093418-75-7
• Molecular Formula: C8H6BrIO2
• Molecular Weight: 340.943
• Hs Code.: 2916399090
• Mol file: 1093418-75-7.mol

Synonyms:4-BroMo-2-iodo-benzoic acid Methyl ester;Methyl 4-bromo-2-iodobenzoate

Chemical Property of 4-BroMo-2-iodo-benzoic acid Methyl ester

Chemical Property:

• Melting Point: <50℃
• Boiling Point: 326.2±27.0 °C(Predicted)
• PSA: 26.30000
• Density: 2.059±0.06 g/cm3(Predicted)
• LogP: 2.84030

Purity/Quality:

97% ^*data from raw suppliers

Methyl4-bromo-2-iodobenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-BroMo-2-iodo-benzoic acid Methyl ester

There total 5 articles about 4-BroMo-2-iodo-benzoic acid Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methanol (67-56-1) + 4-bromo-2- iodobenzoic acid (1133123-02-0) → methyl 4-bromo-2-iodobenzoate (1093418-75-7)

Guidance literature:

With sulfuric acid; In water; at 80 ℃; for 1.5h;

Reference yield: 94.0%

2-amino-4-bromo-benzoic acid methyl ester (135484-83-2) → methyl 4-bromo-2-iodobenzoate (1093418-75-7)

Guidance literature:

2-amino-4-bromo-benzoic acid methyl ester; With sulfuric acid; sodium nitrite; In water; at 0 - 5 ℃; for 0.666667h;

With potassium iodide; In water; at 0 - 5 ℃; for 1h;

Reference yield: 80.0%

4-bromo-2- iodobenzoic acid (1133123-02-0) + methyl iodide (74-88-4) → methyl 4-bromo-2-iodobenzoate (1093418-75-7)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

upstream raw materials:

4-methoxycarbonylphenyl bromide

2-amino-4-bromo-benzoic acid methyl ester

methanol

4-bromo-2- iodobenzoic acid

Downstream raw materials:

methyl 5-bromo-2-(9H-carbazol-9-yl)benzoate

methyl 4-bromo-2-cyanobenzoate

4-bromo-2-cyanobenzoic acid

methyl 4-bromo-2-[(diethoxyphosphoryl)difluoromethyl]benzoate

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