2,6-Diethoxypyridine

Base Information

• Chemical Name: 2,6-Diethoxypyridine
• CAS No.: 13472-57-6
• Molecular Formula: C9H13NO2
• Molecular Weight: 167.208
• Hs Code.: 2933399090
• Mol file: 13472-57-6.mol

Synonyms:2,6-Diethoxypyridine

Chemical Property of 2,6-Diethoxypyridine

Chemical Property:

• Melting Point: 21.5 °C
• Boiling Point: 220.0±20.0 °C(Predicted)
• PKA: 2.84±0.24(Predicted)
• PSA: 31.35000
• Density: 1.021±0.06 g/cm3(Predicted)
• LogP: 1.87900
• Storage Temp.: 2-8°C

Purity/Quality:

99.0% ^*data from raw suppliers

2,6-Diethoxypyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-Diethoxypyridine

There total 4 articles about 2,6-Diethoxypyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2,6-dichloropyridine (2402-78-0) + ethanol (64-17-5) → 2,6-bis(ethoxy)pyridine (13472-57-6)

Guidance literature:

With sodium hydroxide;

Reference yield:

2,6-dichloropyridine (2402-78-0) + sodium ethanolate (141-52-6) → 2,6-bis(ethoxy)pyridine (13472-57-6) + 2-chloro-6-ethoxy-pyridine (42144-78-5)

Guidance literature:

In methanol; ethanol; for 25h; Heating;

Reference yield:

6-ethoxy-2-bromo-pyridine (4645-11-8) + sodium ethanolate (141-52-6) → 2,6-bis(ethoxy)pyridine (13472-57-6)

Guidance literature:

With ethanol; at 160 ℃;

upstream raw materials:

6-ethoxy-2-bromo-pyridine

sodium ethanolate

2,6-dichloropyridine

2,6-Dibromopyridine

Downstream raw materials:

2,6-dihydroxypyridine

2,6-diethoxy-3,5-dibromo-pyridine

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