Methyl 1H-pyrazolo[3,4-c]pyridine-5-carboxylate

Base Information

• Chemical Name: Methyl 1H-pyrazolo[3,4-c]pyridine-5-carboxylate
• CAS No.: 1033772-26-7
• Molecular Formula: C8H7N3O2
• Molecular Weight: 177.162
• Hs Code.: 2933990090
• Mol file: 1033772-26-7.mol

Synonyms:Methyl 1H-pyrazolo[3,4-c]pyridine-5-carboxylate;4-c]pyridine-5-carboxylate;Methyl 1H-pyrazolo[3;Methyl 1H-pyrazolo[3,4-c]...

Chemical Property of Methyl 1H-pyrazolo[3,4-c]pyridine-5-carboxylate

Chemical Property:

• PSA: 67.87000
• LogP: 0.74450
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

Methyl1H-Pyrazolo[3,4-c]pyridine-5-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 1H-pyrazolo[3,4-c]pyridine-5-carboxylate

There total 3 articles about Methyl 1H-pyrazolo[3,4-c]pyridine-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methanol (67-56-1) + 5-iodo-1H-pyrazolo[3,4-c]pyridine (1033772-25-6) + carbon monoxide (201230-82-2) → methyl 1H-pyrazolo[3,4-c]pyridine-5-carboxylate (1033772-26-7)

Guidance literature:

With triethylamine; bis-triphenylphosphine-palladium(II) chloride; In dimethyl sulfoxide; at 105 ℃;

Reference yield: 79.0%

methyl 5-amino-4-methylpyridine-2-carboxylate (868551-99-9) → methyl 1H-pyrazolo[3,4-c]pyridine-5-carboxylate (1033772-26-7)

Guidance literature:

With sodium nitrite; In water; acetic acid; at 20 ℃; for 4h;

Reference yield:

4-methyl-5-nitro-pyridine-2-carboxylic acid methyl ester (868551-30-8) → methyl 1H-pyrazolo[3,4-c]pyridine-5-carboxylate (1033772-26-7)

Guidance literature:

4-methyl-5-nitro-pyridine-2-carboxylic acid methyl ester; With hydrogen; palladium over charcoal; In tetrahydrofuran;

With acetic acid; sodium nitrite;

upstream raw materials:

methyl 5-amino-4-methylpyridine-2-carboxylate

4-methyl-5-nitro-pyridine-2-carboxylic acid methyl ester

methanol

5-iodo-1H-pyrazolo[3,4-c]pyridine

Downstream raw materials:

C₇H₅N₃O₂

methyl 2-(4-fluorobenzyl)-2H-pyrazolo[3,4-c]pyridine-5-carboxylate

methyl 1-(4-fluorobenzyl)-1H-pyrazolo[3,4-c]pyridine-5-carboxylate

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