3-BroMo-N-Methyl-benzeneethanaMine

Base Information

• Chemical Name: 3-BroMo-N-Methyl-benzeneethanaMine
• CAS No.: 785032-26-0
• Molecular Formula: C9H12BrN
• Molecular Weight: 214.105
• Hs Code.: 2921499090
• Mol file: 785032-26-0.mol

Synonyms:3-BroMo-N-Methyl-benzeneethanaMine;N-[2-(3-Bromophenyl)ethyl]-N-methylamine

Chemical Property of 3-BroMo-N-Methyl-benzeneethanaMine

Chemical Property:

• PSA: 12.03000
• LogP: 2.60190

Purity/Quality:

95%-98% ^*data from raw suppliers

N-[2-(3-Bromophenyl)ethyl]-N-methylamine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-BroMo-N-Methyl-benzeneethanaMine

There total 6 articles about 3-BroMo-N-Methyl-benzeneethanaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2-(3-bromophenyl)ethanamine (58971-11-2) → 2-(3-bromophenyl)-N-methylethanamine (785032-26-0)

Guidance literature:

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 90 ℃; for 0.0833333h; Microwave irradiation;

Reference yield: 68.0%

→ 2-(3-bromophenyl)-N-methylethanamine (785032-26-0)

Guidance literature:

Reference yield: 18.32%

formic acid (64-18-6) + 2-(3-bromophenyl)ethanamine (58971-11-2) → 2-(3-bromophenyl)-N-methylethanamine (785032-26-0)

Guidance literature:

formic acid; 2-(3-bromophenyl)ethanamine; With formic acid ethyl ester; for 0.75h; Reflux;

With borane-THF; In tetrahydrofuran; at 0 ℃; for 1h; Reflux;

upstream raw materials:

formaldehyd

2-(3-bromophenyl)ethanamine

1-bromo-3-(2-bromoethyl)benzene

methylamine

Downstream raw materials:

2-(3-bromophenyl)-N,N-dimethylethanamine