1H-Pyrrolo[2,3-b]pyridine, 6-broMo-1-[tris(1-Methylethyl)silyl]-

Base Information

Chemical Name:1H-Pyrrolo[2,3-b]pyridine, 6-broMo-1-[tris(1-Methylethyl)silyl]-
CAS No.:1041181-58-1
Molecular Formula:C16H25BrN2Si
Molecular Weight:353.377
Hs Code.:
Mol file:1041181-58-1.mol

Synonyms:1H-Pyrrolo[2,3-b]pyridine, 6-broMo-1-[tris(1-Methylethyl)silyl]-

Suppliers and Price of 1H-Pyrrolo[2,3-b]pyridine, 6-broMo-1-[tris(1-Methylethyl)silyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Pyrrolo[2,3-b]pyridine, 6-broMo-1-[tris(1-Methylethyl)silyl]-

Chemical Property:

PSA：17.82000
LogP:5.82240

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Pyrrolo[2,3-b]pyridine, 6-broMo-1-[tris(1-Methylethyl)silyl]-

There total 1 articles about 1H-Pyrrolo[2,3-b]pyridine, 6-broMo-1-[tris(1-Methylethyl)silyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 143468-13-7
6-Bromo-1H-pyrrolo<2,3-b>pyridine

: 1041181-58-1
6-bromo-1-(triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; at 55 ℃; for 16h;

Reference yield: 91.0%

: 1041181-58-1
6-bromo-1-(triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridine

: 372-39-4
3,5-difluoroaniline

: 1342812-74-1
N-(3,5-difluorophenyl)-1-(triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridin-6-amine

Guidance literature:: With palladium diacetate; potassium carbonate; XPhos; In tert-butyl alcohol; at 110 ℃; for 3h;
DOI:10.1016/j.bmcl.2017.02.001

Reference yield: 90.0%

: 39512-51-1
1-(o-toluyl)piperazine

: 1041181-58-1
6-bromo-1-(triisopropylsilyl)-1H-pyrrolo[2,3-b]pyridine

: triisopropyl-[6-[4-(o-tolyl)piperazin-1-yl]pyrrolo[2,3-b]pyridin-1-yl]silane

Guidance literature:: With methanesulfonato(2-dicyclohexylphosphino-2’,6’-di-i-propoxy-1,1’-biphenyl)(2’-methylamino-1,1‘-biphenyl-2-yl)palladium(II); sodium t-butanolate; In 1,4-dioxane; at 90 - 110 ℃;