(S)-(4-benzyloxy-phenyl)-tert-butoxycarbonylamino-acetic acid benzyl ester

Base Information

Chemical Name:(S)-(4-benzyloxy-phenyl)-tert-butoxycarbonylamino-acetic acid benzyl ester
CAS No.:914452-19-0
Molecular Formula:C₂₇H₂₉NO₅
Molecular Weight:447.531
Hs Code.:

Synonyms:(S)-(4-benzyloxy-phenyl)-tert-butoxycarbonylamino-acetic acid benzyl ester

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Chemical Property of (S)-(4-benzyloxy-phenyl)-tert-butoxycarbonylamino-acetic acid benzyl ester

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Technology Process of (S)-(4-benzyloxy-phenyl)-tert-butoxycarbonylamino-acetic acid benzyl ester

There total 1 articles about (S)-(4-benzyloxy-phenyl)-tert-butoxycarbonylamino-acetic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 69651-48-5
N-tert-butyloxycarbonyl-L-4-hydroxyphenylglycine

: 100-39-0
benzyl bromide

: 914452-19-0
(S)-(4-benzyloxy-phenyl)-tert-butoxycarbonylamino-acetic acid benzyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 17h;

Reference yield: 44.0%

: 914452-19-0
(S)-(4-benzyloxy-phenyl)-tert-butoxycarbonylamino-acetic acid benzyl ester

: 123593-66-8
L-N-(tert-butoxycarbonyl)-4-benzyloxyphenylglycine

Guidance literature:: (S)-(4-benzyloxy-phenyl)-tert-butoxycarbonylamino-acetic acid benzyl ester; With lithium hydroxide; water; In 1,4-dioxane; at 20 ℃; for 2h;

With hydrogenchloride; In 1,4-dioxane; water; ethyl acetate; pH=3;

Reference yield:

: 914452-19-0
(S)-(4-benzyloxy-phenyl)-tert-butoxycarbonylamino-acetic acid benzyl ester

: (S)-amino-[4-(4-{[(2-hydroxycarbamoyl-benzo[b]thiophen-6-ylrnethyl)-amino]-methyl}-phenoxy)-phenyl]-acetic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hydroxide; water / 1,4-dioxane / 2 h / 20 °C

1.2: pH 3

2.1: pyridine; copper diacetate; triethylamine / dichloromethane / 4.5 h / 20 °C / Molecular sieve

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate

4.1: 1,2-dichloro-ethane / 0.5 h

4.2: 1 h / 20 °C

5.1: hydrogenchloride / 1,4-dioxane; dichloromethane / 0.5 h

With pyridine; hydrogenchloride; lithium hydroxide; water; hydrogen; copper diacetate; triethylamine; palladium 10% on activated carbon; In 1,4-dioxane; dichloromethane; ethyl acetate; 1,2-dichloro-ethane;