tetrakis(trimethylsilyl) (1-amino-1-phenylmethylene)bisphosphonate

Base Information

Chemical Name:tetrakis(trimethylsilyl) (1-amino-1-phenylmethylene)bisphosphonate
CAS No.:1605320-75-9
Molecular Formula:C₁₉H₄₃NO₆P₂Si₄
Molecular Weight:555.843
Hs Code.:

Synonyms:tetrakis(trimethylsilyl) (1-amino-1-phenylmethylene)bisphosphonate

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Chemical Property of tetrakis(trimethylsilyl) (1-amino-1-phenylmethylene)bisphosphonate

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Technology Process of tetrakis(trimethylsilyl) (1-amino-1-phenylmethylene)bisphosphonate

There total 3 articles about tetrakis(trimethylsilyl) (1-amino-1-phenylmethylene)bisphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 100-47-0
benzonitrile

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 1605320-75-9
tetrakis(trimethylsilyl) (1-amino-1-phenylmethylene)bisphosphonate

Guidance literature:: benzonitrile; With phosphorous acid; phosphorus trichloride; In dichloromethane; at 5 - 80 ℃; for 29h;

With water; In dichloromethane; at 80 ℃; for 1h;

1,1,1,3,3,3-hexamethyl-disilazane; Reflux;
DOI:10.1007/s11172-016-1289-z

Reference yield: 72.0%

: 1795-31-9
tris(trimethylsilyl) phosphite

: 5333-86-8
ethyl benzimidate hydrochloride

: 1605320-75-9
tetrakis(trimethylsilyl) (1-amino-1-phenylmethylene)bisphosphonate

Guidance literature:: tris(trimethylsilyl) phosphite; ethyl benzimidate hydrochloride; With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; for 1h; Reflux;

With 1,1,1,3,3,3-hexamethyl-disilazane; for 1h; Reflux;
DOI:10.1134/S1070363214030347

Reference yield: 72.0%

: 1795-31-9
tris(trimethylsilyl) phosphite

: 5333-86-8
ethyl benzimidate hydrochloride

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 1605320-75-9
tetrakis(trimethylsilyl) (1-amino-1-phenylmethylene)bisphosphonate

Guidance literature:: tris(trimethylsilyl) phosphite; ethyl benzimidate hydrochloride; With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 40 ℃; for 1h; Inert atmosphere;

1,1,1,3,3,3-hexamethyl-disilazane; Reflux; Inert atmosphere;
DOI:10.1002/hc.21220