Technology Process of 4,4'-(2,5,8,11,14,17,20,23,26-nonoxaheptacosane-1,27-diyl)dibenzoic acid
There total 3 articles about 4,4'-(2,5,8,11,14,17,20,23,26-nonoxaheptacosane-1,27-diyl)dibenzoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
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1355460-27-3
dimethyl 4,4'-(2,5,8,11,14,17,20,23,26-nonoxaheptacosane-1,27-diyl)dibenzoate
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1355460-32-0
4,4'-(2,5,8,11,14,17,20,23,26-nonoxaheptacosane-1,27-diyl)dibenzoic acid
- Guidance literature:
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dimethyl 4,4'-(2,5,8,11,14,17,20,23,26-nonoxaheptacosane-1,27-diyl)dibenzoate;
With
sodium hydroxide;
In
methanol; water;
for 4h;
Reflux;
With
hydrogenchloride;
In
methanol; water;
DOI:10.1016/j.bmc.2011.10.063
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1355460-32-0
4,4'-(2,5,8,11,14,17,20,23,26-nonoxaheptacosane-1,27-diyl)dibenzoic acid
- Guidance literature:
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Multi-step reaction with 2 steps
1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0 °C
1.2: 2 h / 20 °C
2.1: sodium hydroxide / methanol; water / 4 h / Reflux
With
potassium hexamethylsilazane; sodium hydroxide;
In
tetrahydrofuran; methanol; water; toluene;
DOI:10.1016/j.bmc.2011.10.063
-
-
1355460-32-0
4,4'-(2,5,8,11,14,17,20,23,26-nonoxaheptacosane-1,27-diyl)dibenzoic acid
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0 °C
1.2: 2 h / 20 °C
2.1: sodium hydroxide / methanol; water / 4 h / Reflux
With
potassium hexamethylsilazane; sodium hydroxide;
In
tetrahydrofuran; methanol; water; toluene;
DOI:10.1016/j.bmc.2011.10.063
