(R)-((S)-4,4-dimethyl-2-oxotetrahydrofuran-3-yl) 4-methylcyclohex-3-ene carboxylate

Base Information

Chemical Name:(R)-((S)-4,4-dimethyl-2-oxotetrahydrofuran-3-yl) 4-methylcyclohex-3-ene carboxylate
CAS No.:1384122-49-9
Molecular Formula:C₁₄H₂₀O₄
Molecular Weight:252.31
Hs Code.:

Synonyms:(R)-((S)-4,4-dimethyl-2-oxotetrahydrofuran-3-yl) 4-methylcyclohex-3-ene carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-((S)-4,4-dimethyl-2-oxotetrahydrofuran-3-yl) 4-methylcyclohex-3-ene carboxylate

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Technology Process of (R)-((S)-4,4-dimethyl-2-oxotetrahydrofuran-3-yl) 4-methylcyclohex-3-ene carboxylate

There total 3 articles about (R)-((S)-4,4-dimethyl-2-oxotetrahydrofuran-3-yl) 4-methylcyclohex-3-ene carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 127604-93-7
(S)-4,4-dimethyl-2-oxotetrahydrofuran-3-yl acrylate

: 78-79-5,9003-31-0
isoprene

: 1384122-49-9
(R)-((S)-4,4-dimethyl-2-oxotetrahydrofuran-3-yl) 4-methylcyclohex-3-ene carboxylate

Guidance literature:: (S)-4,4-dimethyl-2-oxotetrahydrofuran-3-yl acrylate; With titanium tetrachloride; In hexane; dichloromethane; at -10 ℃; for 0.25h;

isoprene; In hexane; dichloromethane; at -10 - 0 ℃; for 5.58h;

Reference yield:

: 79-50-5,599-04-2,5405-40-3,52126-90-6
(S)-pantolactone

: 1384122-49-9
(R)-((S)-4,4-dimethyl-2-oxotetrahydrofuran-3-yl) 4-methylcyclohex-3-ene carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / -10 °C

2: titanium tetrachloride / dichloromethane; water; ethyl acetate

With titanium tetrachloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; ethyl acetate;

Reference yield:

: 1384122-49-9
(R)-((S)-4,4-dimethyl-2-oxotetrahydrofuran-3-yl) 4-methylcyclohex-3-ene carboxylate

Guidance literature:: With titanium tetrachloride; In hexane; dichloromethane; at -10 ℃; for 0.25h;

In hexane; dichloromethane; at -10 - 0 ℃; for 4.08333h;