(1R)-4-methylcyclohex-3-enecarboxylic acid chloride

Base Information

Chemical Name:(1R)-4-methylcyclohex-3-enecarboxylic acid chloride
CAS No.:1314795-37-3
Molecular Formula:C₈H₁₁ClO
Molecular Weight:158.628
Hs Code.:

Synonyms:(1R)-4-methylcyclohex-3-enecarboxylic acid chloride

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Chemical Property of (1R)-4-methylcyclohex-3-enecarboxylic acid chloride

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Technology Process of (1R)-4-methylcyclohex-3-enecarboxylic acid chloride

There total 5 articles about (1R)-4-methylcyclohex-3-enecarboxylic acid chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 121424-36-0
(+)-(1R)-4-methyl-cyclohex-3-enecarboxylic acid

: 1314795-37-3
(1R)-4-methylcyclohex-3-enecarboxylic acid chloride

Guidance literature:: With potassium phosphate; oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; for 1h;
DOI:10.1021/jm401420j

Reference yield:

: 1384122-49-9
(R)-((S)-4,4-dimethyl-2-oxotetrahydrofuran-3-yl) 4-methylcyclohex-3-ene carboxylate

: 1314795-37-3
(1R)-4-methylcyclohex-3-enecarboxylic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: water; lithium hydroxide / tetrahydrofuran; methanol / 1 h / 50 °C

2: potassium phosphate; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 0 - 20 °C

With potassium phosphate; oxalyl dichloride; water; N,N-dimethyl-formamide; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 78-79-5,9003-31-0
isoprene

: 1314795-37-3
(1R)-4-methylcyclohex-3-enecarboxylic acid chloride

Guidance literature:: Multi-step reaction with 3 steps

1: titanium tetrachloride / dichloromethane / -10 - -9 °C / Large scale

2: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 - 27 °C / Large scale

3: potassium phosphate; N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2 h / 0 - 20 °C

With potassium phosphate; oxalyl dichloride; lithium hydroxide monohydrate; water; titanium tetrachloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; 1: |Diels-Alder Cycloaddition;