Mes₂HPCH₂CH₂BCl(C₆F₅)2

Base Information

• Chemical Name: Mes₂HPCH₂CH₂BCl(C₆F₅)2
• CAS No.: 1403338-72-6
• Molecular Formula: C₃₂H₂₆BClF₁₀P*H
• Molecular Weight: 678.788
• Mol file: 1403338-72-6.mol

Synonyms:Mes₂HPCH₂CH₂BCl(C₆F₅)2

Chemical Property of Mes₂HPCH₂CH₂BCl(C₆F₅)2

Chemical Property:

Purity/Quality:

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Technology Process of Mes₂HPCH₂CH₂BCl(C₆F₅)2

There total 17 articles about Mes₂HPCH₂CH₂BCl(C₆F₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

[2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane (1003010-59-0) → Mes2HPCH2CH2BCl(C6F5)2 (1403338-72-6)

Guidance literature:

With hydrogenchloride; In diethyl ether; benzene; Inert atmosphere;

DOI:10.1002/ejic.201200288

Reference yield:

[2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane (1003010-59-0) → Mes2ClPCH2CH2BCl(C6F5)2 (1403338-68-0) + Mes2HPCH2CH2BCl(C6F5)2 (1403338-72-6)

Guidance literature:

With chlorine; In pentane; at 20 ℃; for 5.16667h; Inert atmosphere;

DOI:10.1002/ejic.201200288

Reference yield:

bis(pentafluorophenyl)borohydride (165612-94-2) → Mes2HPCH2CH2BCl(C6F5)2 (1403338-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / Inert atmosphere

2: hydrogenchloride / diethyl ether; benzene / Inert atmosphere

With hydrogenchloride; In diethyl ether; benzene;

DOI:10.1002/ejic.201200288

upstream raw materials:

dimesitylvinylphosphine

[2-(dimesitylphosphino)ethyl]bis(pentafluorophenyl)borane

bis(pentafluorophenyl)borohydride

hydrogenchloride