Technology Process of C67H62Cl2N8O16P2
There total 6 articles about C67H62Cl2N8O16P2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1-mesitylenesulfonyl-4-nitroimidazole;
In
pyridine;
at 30 ℃;
for 16h;
DOI:10.1248/cpb.29.3440
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 73 percent / diethyl ether; benzene / 6 h / Ambient temperature
2: 98 percent / 1-methyl imidazole / dioxane / 2 h / 25 °C
3: 2 percent benzene-sulfonic acid / CH2Cl2; methanol / 0.25 h / 0 °C
4: 92 percent / MSNI / pyridine / 16 h / 30 °C
With
1-methyl-1H-imidazole; benzenesulfonic acid; 1-mesitylenesulfonyl-4-nitroimidazole;
In
1,4-dioxane; pyridine; methanol; diethyl ether; dichloromethane; benzene;
DOI:10.1248/cpb.29.3440
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 73 percent / diethyl ether; benzene / 6 h / Ambient temperature
2: 98 percent / 1-methyl imidazole / dioxane / 2 h / 25 °C
3: 2 percent benzene-sulfonic acid / CH2Cl2; methanol / 0.25 h / 0 °C
4: 92 percent / MSNI / pyridine / 16 h / 30 °C
With
1-methyl-1H-imidazole; benzenesulfonic acid; 1-mesitylenesulfonyl-4-nitroimidazole;
In
1,4-dioxane; pyridine; methanol; diethyl ether; dichloromethane; benzene;
DOI:10.1248/cpb.29.3440