7-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylheptanoic acid

Base Information

Chemical Name:7-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylheptanoic acid
CAS No.:868836-02-6
Molecular Formula:C₂₆H₄₃N₃O₅
Molecular Weight:477.645
Hs Code.:

Synonyms:7-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylheptanoic acid

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Chemical Property of 7-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylheptanoic acid

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Technology Process of 7-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylheptanoic acid

There total 5 articles about 7-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylheptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.3%

: 868835-97-6
7-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylheptanoic acid methyl ester

: 868836-02-6
7-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylheptanoic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/jm0505009

Reference yield: 72.3%

: 868836-02-6
7-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylheptanoic acid

Guidance literature:

Reference yield:

: 868835-94-3
1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-aminobutylamine

: 868836-02-6
7-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylheptanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 76.5 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

2: 72.3 percent / aq. LiOH / tetrahydrofuran / 0 - 20 °C

With lithium hydroxide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm0505009