(phenylsulfanyl)(phenyl)diazene

Base Information

• Chemical Name: (phenylsulfanyl)(phenyl)diazene
• CAS No.: 42401-63-8
• Molecular Formula: C₁₂H₁₀N₂S
• Molecular Weight: 214.291
• Mol file: 42401-63-8.mol

Synonyms:(phenylsulfanyl)(phenyl)diazene

Chemical Property of (phenylsulfanyl)(phenyl)diazene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (phenylsulfanyl)(phenyl)diazene

There total 2 articles about (phenylsulfanyl)(phenyl)diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium thiophenolate (930-69-8) + benzenediazonium o-benzenedisulfonimide → (phenylsulfanyl)(phenyl)diazene (42401-63-8) + diphenyl sulfide (139-66-2) + diphenyldisulfane (882-33-7) + sodium o-benzenedisulfonimide

Guidance literature:

In dimethyl sulfoxide; at 20 - 25 ℃; Further Variations:; Solvents; Temperatures; reaction times; Product distribution;

DOI:10.1021/jo0003347

Reference yield:

benzene diazonium chloride (100-34-5) + thiophenol (108-98-5) → (phenylsulfanyl)(phenyl)diazene (42401-63-8)

Guidance literature:

With water;

Reference yield: 33.0%

(phenylsulfanyl)(phenyl)diazene (42401-63-8) → diphenyl sulfide (139-66-2) + benzonitrile (100-47-0)

Guidance literature:

With tetra-n-butylammonium cyanide; In dimethyl sulfoxide; at 25 ℃; for 1h; Yields of byproduct given; Irradiation;

DOI:10.1016/S0040-4020(01)86905-2

upstream raw materials:

benzene diazonium chloride

thiophenol

sodium thiophenolate

Downstream raw materials:

diphenyl sulfide

benzonitrile

benzene

benzene diazonium chloride

Refernces