Technology Process of C27H30ClNO5S
There total 6 articles about C27H30ClNO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium bis[bis(diphenylphosphino)ferrocene] dichloride; caesium carbonate;
In
tetrahydrofuran; water;
at 160 ℃;
for 0.166667h;
Microwave irradiation;
DOI:10.1016/j.bmcl.2011.02.077
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium hydroxide / ethyl acetate
2: palladium bis[bis(diphenylphosphino)ferrocene] dichloride; caesium carbonate / tetrahydrofuran; water / 0.17 h / 160 °C / Microwave irradiation
With
palladium bis[bis(diphenylphosphino)ferrocene] dichloride; caesium carbonate; lithium hydroxide;
In
tetrahydrofuran; water; ethyl acetate;
DOI:10.1016/j.bmcl.2011.02.077
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / 16 h
2: potassium carbonate / N,N-dimethyl-formamide / 0.12 h / 170 °C / Microwave irradiation
3: lithium hydroxide / ethyl acetate
4: palladium bis[bis(diphenylphosphino)ferrocene] dichloride; caesium carbonate / tetrahydrofuran; water / 0.17 h / 160 °C / Microwave irradiation
With
pyridine; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium carbonate; caesium carbonate; lithium hydroxide;
In
tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.02.077
