t-2-<(E)-2'-(2,6-dichlorophenyl)ethen-1'-yl>-r-3-(2,6-dichlorophenyl)oxirane

Base Information

Chemical Name:t-2-<(E)-2'-(2,6-dichlorophenyl)ethen-1'-yl>-r-3-(2,6-dichlorophenyl)oxirane
CAS No.:90281-06-4
Molecular Formula:C₁₆H₁₀Cl₄O
Molecular Weight:360.067
Hs Code.:

Synonyms:t-2-<(E)-2'-(2,6-dichlorophenyl)ethen-1'-yl>-r-3-(2,6-dichlorophenyl)oxirane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of t-2-<(E)-2'-(2,6-dichlorophenyl)ethen-1'-yl>-r-3-(2,6-dichlorophenyl)oxirane

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Technology Process of t-2-<(E)-2'-(2,6-dichlorophenyl)ethen-1'-yl>-r-3-(2,6-dichlorophenyl)oxirane

There total 5 articles about t-2-<(E)-2'-(2,6-dichlorophenyl)ethen-1'-yl>-r-3-(2,6-dichlorophenyl)oxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 89970-57-0
C₁₆H₁₀Cl₄

: 90281-06-4
t-2-<(E)-2'-(2,6-dichlorophenyl)ethen-1'-yl>-r-3-(2,6-dichlorophenyl)oxirane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1.) refrigerator, 24 h; 2.) 5 d, r.t.; excess of m-chloroperbenzoic acid;
DOI:10.1016/0040-4020(84)85121-2

Reference yield:

: 83-38-5
2,6-dichlorobenzaldehyde

: 90281-06-4
t-2-<(E)-2'-(2,6-dichlorophenyl)ethen-1'-yl>-r-3-(2,6-dichlorophenyl)oxirane

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / benzene / 24 h / Heating

2: 83 percent / 50 percent aq. NaOH / CH₂Cl₂; H₂O / 0.67 h

3: 85 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1.) refrigerator, 24 h; 2.) 5 d, r.t.; excess of m-chloroperbenzoic acid

With sodium hydroxide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; benzene;
DOI:10.1016/0040-4020(84)85121-2

Reference yield:

: 18583-54-5
(2,6-dichlorobenzyl)triphenylphosphonium chloride

: 90281-06-4
t-2-<(E)-2'-(2,6-dichlorophenyl)ethen-1'-yl>-r-3-(2,6-dichlorophenyl)oxirane

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / 50 percent aq. NaOH / CH₂Cl₂; H₂O / 0.67 h

2: 85 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1.) refrigerator, 24 h; 2.) 5 d, r.t.; excess of m-chloroperbenzoic acid

With sodium hydroxide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water;
DOI:10.1016/0040-4020(84)85121-2