ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]-3-fluorophenyl}3-ethoxypropanoate

Base Information

Chemical Name:ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]-3-fluorophenyl}3-ethoxypropanoate
CAS No.:1202577-53-4
Molecular Formula:C₂₀H₂₁Cl₂FO₄
Molecular Weight:415.289
Hs Code.:

Synonyms:ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]-3-fluorophenyl}3-ethoxypropanoate

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Chemical Property of ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]-3-fluorophenyl}3-ethoxypropanoate

Chemical Property:

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Technology Process of ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]-3-fluorophenyl}3-ethoxypropanoate

There total 4 articles about ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]-3-fluorophenyl}3-ethoxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1202577-52-3
ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]-3-fluorophenyl}-3-hydroxypropanoate

: 75-03-6
ethyl iodide

: 1202577-53-4
ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]-3-fluorophenyl}3-ethoxypropanoate

Guidance literature:: With silver(l) oxide; In toluene; at 20 - 110 ℃; Inert atmosphere;

Reference yield:

: 405-05-0
3-fluoro-4-hydroxybenzaldehyde

: 1202577-53-4
ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]-3-fluorophenyl}3-ethoxypropanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C

3.1: silver(l) oxide / toluene / 20 - 110 °C / Inert atmosphere

With triphenylphosphine; silver(l) oxide; lithium diisopropyl amide; diethylazodicarboxylate; In tetrahydrofuran; toluene;

Reference yield:

: 1805-32-9
3,4-dichlorobenzyl alcohol

: 1202577-53-4
ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]-3-fluorophenyl}3-ethoxypropanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C

3.1: silver(l) oxide / toluene / 20 - 110 °C / Inert atmosphere

With triphenylphosphine; silver(l) oxide; lithium diisopropyl amide; diethylazodicarboxylate; In tetrahydrofuran; toluene;