(E)-N-[(2S)-1-methoxy-3-methylbutan-2-yl]-1-[(2R)-2-ethylpyridin-1(2H)-yl]-1-phenylmethanimine

Base Information

Chemical Name:(E)-N-[(2S)-1-methoxy-3-methylbutan-2-yl]-1-[(2R)-2-ethylpyridin-1(2H)-yl]-1-phenylmethanimine
CAS No.:386253-33-4
Molecular Formula:C₂₀H₂₈N₂O
Molecular Weight:312.455
Hs Code.:

Synonyms:(E)-N-[(2S)-1-methoxy-3-methylbutan-2-yl]-1-[(2R)-2-ethylpyridin-1(2H)-yl]-1-phenylmethanimine

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Chemical Property of (E)-N-[(2S)-1-methoxy-3-methylbutan-2-yl]-1-[(2R)-2-ethylpyridin-1(2H)-yl]-1-phenylmethanimine

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Technology Process of (E)-N-[(2S)-1-methoxy-3-methylbutan-2-yl]-1-[(2R)-2-ethylpyridin-1(2H)-yl]-1-phenylmethanimine

There total 6 articles about (E)-N-[(2S)-1-methoxy-3-methylbutan-2-yl]-1-[(2R)-2-ethylpyridin-1(2H)-yl]-1-phenylmethanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 110-86-1
pyridine

: 557-20-0
diethylzinc

: 87768-46-5
N-[(1S)-1-(methoxymethyl)-2-methylpropyl]benzamide

: [1-(4-Ethyl-4H-pyridin-1-yl)-1-phenyl-meth-(E)-ylidene]-((S)-1-methoxymethyl-2-methyl-propyl)-amine

: 386253-33-4
(E)-N-[(2S)-1-methoxy-3-methylbutan-2-yl]-1-[(2R)-2-ethylpyridin-1(2H)-yl]-1-phenylmethanimine

Guidance literature:: pyridine; N-[(1S)-1-(methoxymethyl)-2-methylpropyl]benzamide; With trifluoromethylsulfonic anhydride; In dichloromethane; at -40 - 20 ℃; for 1h;

diethylzinc; In dichloromethane; at -20 ℃; for 3h;
DOI:10.1021/ja017136x

Reference yield:

: 1185294-54-5
1-(1-methylethoxy)-3-phenyl-2-propylamine hydrochloride

: 386253-33-4
(E)-N-[(2S)-1-methoxy-3-methylbutan-2-yl]-1-[(2R)-2-ethylpyridin-1(2H)-yl]-1-phenylmethanimine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / triethylamine / CH₂Cl₂ / 0 °C

2: CH₂Cl₂ / -40 - 25 °C

3: CH₂Cl₂; diethyl ether / -78 °C

With triethylamine; In diethyl ether; dichloromethane;
DOI:10.1021/ja017136x

Reference yield:

: 98-88-4
benzoyl chloride

: 386253-33-4
(E)-N-[(2S)-1-methoxy-3-methylbutan-2-yl]-1-[(2R)-2-ethylpyridin-1(2H)-yl]-1-phenylmethanimine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / triethylamine / CH₂Cl₂ / 0 °C

2: CH₂Cl₂ / -40 - 25 °C

3: CH₂Cl₂; diethyl ether / -78 °C

With triethylamine; In diethyl ether; dichloromethane;
DOI:10.1021/ja017136x