(S)-4-Benzyl-3-[4-(2-methyl-[1,3]dithian-2-yl)-butyryl]-oxazolidin-2-one

Base Information

Chemical Name:(S)-4-Benzyl-3-[4-(2-methyl-[1,3]dithian-2-yl)-butyryl]-oxazolidin-2-one
CAS No.:287717-24-2
Molecular Formula:C₁₉H₂₅NO₃S₂
Molecular Weight:379.544
Hs Code.:

Synonyms:(S)-4-Benzyl-3-[4-(2-methyl-[1,3]dithian-2-yl)-butyryl]-oxazolidin-2-one

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Chemical Property of (S)-4-Benzyl-3-[4-(2-methyl-[1,3]dithian-2-yl)-butyryl]-oxazolidin-2-one

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Technology Process of (S)-4-Benzyl-3-[4-(2-methyl-[1,3]dithian-2-yl)-butyryl]-oxazolidin-2-one

There total 2 articles about (S)-4-Benzyl-3-[4-(2-methyl-[1,3]dithian-2-yl)-butyryl]-oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 109-80-8
1.3-propanedithiol

: 273753-64-3
1-(4(S)-Benzyl-2-oxo-oxazolidin-3-yl)-hexane-1,5-dione

: 287717-24-2
(S)-4-Benzyl-3-[4-(2-methyl-[1,3]dithian-2-yl)-butyryl]-oxazolidin-2-one

Guidance literature:: With toluene-4-sulfonic acid; In acetic acid;
DOI:10.1016/S0040-4039(00)00504-9

Reference yield:

: 134916-00-0
(4S)-4-benzyl-3-(hex-5-enoyl)-1,3-oxazolidin-2-one

: 287717-24-2
(S)-4-Benzyl-3-[4-(2-methyl-[1,3]dithian-2-yl)-butyryl]-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / O₂; copper (I) chloride; palladium (II) chloride / dimethylformamide; H₂O

2: 98 percent / p-toluenesulfonic acid / acetic acid / 0.5 h

With oxygen; toluene-4-sulfonic acid; copper(l) chloride; palladium dichloride; In water; acetic acid; N,N-dimethyl-formamide; 1: Wacker oxidation;
DOI:10.1021/ja020091v

Reference yield: 72.0%

: 79-03-8
propionyl chloride

: 287717-24-2
(S)-4-Benzyl-3-[4-(2-methyl-[1,3]dithian-2-yl)-butyryl]-oxazolidin-2-one

: 287717-25-3
(R)-1-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-2-[2-(2-methyl-[1,3]dithian-2-yl)-ethyl]-pentane-1,3-dione

: Propionic acid (Z)-1-((S)-4-benzyl-2-oxo-oxazolidin-3-yl)-4-(2-methyl-[1,3]dithian-2-yl)-but-1-enyl ester

Guidance literature:: (S)-4-Benzyl-3-[4-(2-methyl-[1,3]dithian-2-yl)-butyryl]-oxazolidin-2-one; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1.5h;

propionyl chloride; In tetrahydrofuran; at -78 ℃; for 0.166667h; Further stages.;
DOI:10.1021/ja020091v