C₁₅H₁₆Cl₂N₄O₃

Base Information

Chemical Name:C₁₅H₁₆Cl₂N₄O₃
CAS No.:1352798-46-9
Molecular Formula:C₁₅H₁₆Cl₂N₄O₃
Molecular Weight:371.223
Hs Code.:

C<sub>15</sub>H<sub>16</sub>Cl<sub>2</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:C₁₅H₁₆Cl₂N₄O₃

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Chemical Property of C₁₅H₁₆Cl₂N₄O₃

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Technology Process of C₁₅H₁₆Cl₂N₄O₃

There total 5 articles about C₁₅H₁₆Cl₂N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39183-17-0
4-hydroxy-2,3-dichloroaniline

: 1352798-46-9
C₁₅H₁₆Cl₂N₄O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere

1.2: 19 h / 20 °C

2.1: iron; acetic acid / 1.5 h / 55 °C

3.1: pyridine / tetrahydrofuran / 1.58 h / 0 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 °C / Inert atmosphere

4.2: 78.5 h / 0 °C

With pyridine; iron; sodium hydride; potassium carbonate; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1352798-56-1
ethyl (2-amino-4-(4-amino-2,3-dichlorophenoxy)pyridin-3-yl)carbamate

: 74-88-4
methyl iodide

: 1352798-46-9
C₁₅H₁₆Cl₂N₄O₃

Guidance literature:: ethyl (2-amino-4-(4-amino-2,3-dichlorophenoxy)pyridin-3-yl)carbamate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.75h; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 78.5h;

Reference yield:

: 6980-08-1
4-chloro-3-nitro-2-pyridinamine

: 1352798-46-9
C₁₅H₁₆Cl₂N₄O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere

1.2: 19 h / 20 °C

2.1: iron; acetic acid / 1.5 h / 55 °C

3.1: pyridine / tetrahydrofuran / 1.58 h / 0 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 °C / Inert atmosphere

4.2: 78.5 h / 0 °C

With pyridine; iron; sodium hydride; potassium carbonate; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;