C₅₂H₆₂O₁₄Si

Base Information

Chemical Name:C₅₂H₆₂O₁₄Si
CAS No.:260245-86-1
Molecular Formula:C₅₂H₆₂O₁₄Si
Molecular Weight:939.141
Hs Code.:

C<sub>52</sub>H<sub>62</sub>O<sub>14</sub>Si

Synonyms:C₅₂H₆₂O₁₄Si

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Chemical Property of C₅₂H₆₂O₁₄Si

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Technology Process of C₅₂H₆₂O₁₄Si

There total 1 articles about C₅₂H₆₂O₁₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 160237-44-5
C₄₃H₅₆O₁₂Si

: 260245-86-1
C₅₂H₆₂O₁₄Si

Guidance literature:: at 90 ℃; for 3h; under 1 Torr;
DOI:10.1016/S0040-4039(99)02055-9

Reference yield: 100.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 260245-86-1
C₅₂H₆₂O₁₄Si

: 260249-46-5
C₅₉H₆₉NO₁₄Si

Guidance literature:: In pyridine; at 20 ℃; for 3h;
DOI:10.1016/S0040-4039(99)02056-0

Reference yield:

: 260245-86-1
C₅₂H₆₂O₁₄Si

: 33069-62-4
taxol

Guidance literature:: Multi-step reaction with 11 steps

1: 100 percent / pyridine / 3 h / 20 °C

2: TsN₃; Et₃N; DBU / acetonitrile / 16 h / 20 °C

3: 80 percent / Cu(acac)2 / 70 h / 60 °C

4: ([Bu]2Sn(Cl))2O / ethanol / 24 h / Heating

5: 90 percent

6: 73 percent / NaBH₃CN / acetic acid

7: HCO₂NH₄ / 10 percent Pd/C / acetic acid / 3 h / 20 °C

8: aq. NaHCO₃ / 3 h / 20 °C

9: 87 percent / DEAD; PPh₃ / 1 h / 0 °C

10: DMAP / pyridine

11: 0.1 N HCl / methanol / 3 h / 60 °C

With hydrogenchloride; dmap; copper acetylacetonate; 4-toluenesulfonyl azide; ammonium formate; 1,3-dichlorotetrabutyldistannoxane; sodium cyanoborohydride; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In pyridine; methanol; ethanol; acetic acid; acetonitrile; 1: Condensation / 2: Diazotization / 3: Substitution / 4: transesterification / 5: Swern oxid. / 6: Reduction / 7: Reduction / 8: Acylation / 9: Dehydration / 10: Acetylation / 11: Hydrolysis;
DOI:10.1016/S0040-4039(99)02056-0