3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-2'-piperazino-2',3'-secouridine

Base Information

Chemical Name:3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-2'-piperazino-2',3'-secouridine
CAS No.:1120329-65-8
Molecular Formula:C₄₀H₅₄N₄O₇Si
Molecular Weight:730.977
Hs Code.:

Synonyms:3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-2'-piperazino-2',3'-secouridine

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Chemical Property of 3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-2'-piperazino-2',3'-secouridine

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Technology Process of 3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-2'-piperazino-2',3'-secouridine

There total 1 articles about 3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-2'-piperazino-2',3'-secouridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-85-0
piperazine

: 1120329-64-7
C₃₇H₄₈N₂O₁₀SSi

: 1120329-65-8
3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-2'-piperazino-2',3'-secouridine

Guidance literature:: In ethanol; at 100 ℃; for 2h;
DOI:10.1021/jo9019978

Reference yield: 89.0%

: 1120329-65-8
3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-2'-piperazino-2',3'-secouridine

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1333413-08-3
3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-2'-(4-(9-fluorenylmethoxycarbonyl)piperazino)-2',3'-secouridine

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.06.087

Reference yield: 83.0%

: 1120329-65-8
3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-2'-piperazino-2',3'-secouridine

: 359858-14-3
6-(2,2′:6′,2″-terpyridine-4′-yloxy)hexanoic acid

: 1197336-31-4
3'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityl)-2'-(4-(6-((2,2':6',2''-terpyridin-4'-yl)oxy)hexanoyl)-piperazino)-2',3'-secouridine

Guidance literature:: 6-(2,2′:6′,2″-terpyridine-4′-yloxy)hexanoic acid; With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 0.583333h;

3'-O-tert-butyldimethylsilyl-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-2'-piperazino-2',3'-secouridine; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h;
DOI:10.1021/jo9019978