N'-cyclopentylidene-2-hydroxybenzohydrazide

Base Information

Chemical Name:N'-cyclopentylidene-2-hydroxybenzohydrazide
CAS No.:100135-10-2
Molecular Formula:C₁₂H₁₄N₂O₂
Molecular Weight:218.255
Hs Code.:
Mol file:100135-10-2.mol

Synonyms:N'-cyclopentylidene-2-hydroxybenzohydrazide

Suppliers and Price of N'-cyclopentylidene-2-hydroxybenzohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Aronis compounds
N'-cyclopentylidene-2-hydroxybenzohydrazide
50mg
$ 50.00

Aronis compounds
N'-cyclopentylidene-2-hydroxybenzohydrazide
5mg
$ 15.00

Total 0 raw suppliers

Chemical Property of N'-cyclopentylidene-2-hydroxybenzohydrazide

Chemical Property:

Purity/Quality:: N'-cyclopentylidene-2-hydroxybenzohydrazide ^*data from reagent suppliers

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Technology Process of N'-cyclopentylidene-2-hydroxybenzohydrazide

There total 1 articles about N'-cyclopentylidene-2-hydroxybenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 936-02-7
2-Hydroxybenzoylhydrazine

: 120-92-3
cyclopentanone

: 100135-10-2
N'-cyclopentylidene-2-hydroxybenzohydrazide

Guidance literature:: at 114 ℃; for 0.0833333h; under 1425.14 Torr; Microwave irradiation; neat (no solvent);
DOI:10.1021/cc9001444

Reference yield: 95.0%

: 100135-10-2
N'-cyclopentylidene-2-hydroxybenzohydrazide

: 7705-08-0
iron(III) chloride

: [Fe2(N-cyclopentylidene-2-hydroxybenzohydrazinde-1H)4(μ-OCH3)2]

Guidance literature:: With sodium acetate; In methanol; methanolic sol. of FeCl3 added dropwise to well stirred soln. of ligand in MeOH and then to mixt. added dropwise soln. of sodium acetate in MeOHand soln. stirred for 6 h at room temp.; ppt. filtered off, rinsed with MeOH and dried in vac.; elem. anal.;
DOI:10.1016/j.ica.2009.08.027

Reference yield: 30.0%

: 67-56-1
methanol

: 100135-10-2
N'-cyclopentylidene-2-hydroxybenzohydrazide

: 7705-08-0
iron(III) chloride

: 1220836-48-5
[FeCl₂(HOC₆H₄C(O)NHNC₅H₈)2]*CH₃OH

Guidance literature:: In methanol; N2; ligand (0.3 mmol) mixed with FeCl3 (0.1 mmol) in MeOH, stirred at room temp. for 6 h; layered (Et2O), crystd. on storage for 2-4 d, filtered off, washed (Et2O), elem. anal.;
DOI:10.1002/ejic.200900382