3,5-dichlorobenzyl 4-(2-((tert-butoxycarbonyl)amino)ethyl)piperidine-1-carboxylate

Base Information

Chemical Name:3,5-dichlorobenzyl 4-(2-((tert-butoxycarbonyl)amino)ethyl)piperidine-1-carboxylate
CAS No.:1613512-87-0
Molecular Formula:C₂₀H₂₈Cl₂N₂O₄
Molecular Weight:431.359
Hs Code.:

Synonyms:3,5-dichlorobenzyl 4-(2-((tert-butoxycarbonyl)amino)ethyl)piperidine-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-dichlorobenzyl 4-(2-((tert-butoxycarbonyl)amino)ethyl)piperidine-1-carboxylate

Chemical Property:

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Technology Process of 3,5-dichlorobenzyl 4-(2-((tert-butoxycarbonyl)amino)ethyl)piperidine-1-carboxylate

There total 2 articles about 3,5-dichlorobenzyl 4-(2-((tert-butoxycarbonyl)amino)ethyl)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1175526-48-3
3,5-dichlorobenzyl carbonochloridate

: 165528-81-4
tert-butyl 2-(piperidin-4-yl)ethylcarbamate

: 1613512-87-0
3,5-dichlorobenzyl 4-(2-((tert-butoxycarbonyl)amino)ethyl)piperidine-1-carboxylate

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/j.bmcl.2018.05.030

Reference yield:

: 1175526-48-3
3,5-dichlorobenzyl carbonochloridate

: 144-55-8
sodium hydrogencarbonate

: 165528-81-4
tert-butyl 2-(piperidin-4-yl)ethylcarbamate

: 1613512-87-0
3,5-dichlorobenzyl 4-(2-((tert-butoxycarbonyl)amino)ethyl)piperidine-1-carboxylate

Guidance literature:

Reference yield: 75.0%

: 1613512-87-0
3,5-dichlorobenzyl 4-(2-((tert-butoxycarbonyl)amino)ethyl)piperidine-1-carboxylate

: 74-88-4
methyl iodide

: 1613512-88-1
3,5-dichlorobenzyl 4-(2-((tert-butoxycarbonyl)(methyl)amino)ethyl)piperidine-1-carboxylate

Guidance literature:: 3,5-dichlorobenzyl 4-(2-((tert-butoxycarbonyl)amino)ethyl)piperidine-1-carboxylate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; for 0.25h; Cooling with ice;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; for 5h;
DOI:10.1016/j.bmcl.2018.05.030