C₂₂H₃₁N₃O₅

Base Information

Chemical Name:C₂₂H₃₁N₃O₅
CAS No.:1425940-85-7
Molecular Formula:C₂₂H₃₁N₃O₅
Molecular Weight:417.505
Hs Code.:

C<sub>22</sub>H<sub>31</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₂₂H₃₁N₃O₅

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Chemical Property of C₂₂H₃₁N₃O₅

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Technology Process of C₂₂H₃₁N₃O₅

There total 6 articles about C₂₂H₃₁N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1425940-84-6
(S)-methyl-2-methyl-2-(2-(pyrrolidine-2-carboxamido)benzamido)propanoate

: 3282-30-2
pivaloyl chloride

: 1425940-85-7
C₂₂H₃₁N₃O₅

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 5h;
DOI:10.1021/ol4002762

Reference yield:

: 221539-54-4
N-(2-aminobenzoyl)-α-methylalanine methyl ester

: 1425940-85-7
C₂₂H₃₁N₃O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 0.42 h / 0 °C / Inert atmosphere

1.2: 8 h / Inert atmosphere; Reflux

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C

With chloroformic acid ethyl ester; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol4002762

Reference yield:

: 610-14-0
2-nitrobenzyl chloride

: 1425940-85-7
C₂₂H₃₁N₃O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 5 h / 20 °C / Cooling with ice

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 5 h / 3102.97 Torr

3.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 0.42 h / 0 °C / Inert atmosphere

3.2: 8 h / Inert atmosphere; Reflux

4.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

5.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C

With palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1021/ol4002762