3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptonic acid

Base Information

Chemical Name:3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptonic acid
CAS No.:260551-08-4
Molecular Formula:C₃₀H₃₃NO₇
Molecular Weight:519.595
Hs Code.:

Synonyms:3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptonic acid

Suppliers and Price of 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptonic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptonic acid

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptonic acid

There total 7 articles about 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 768385-13-3
(2-acetamido-3,4,6-tri-O-benzyl-1,2-dideoxy-α-D-glucopyranosyl) cyanide

: 260551-08-4
3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptonic acid

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; water; at 60 ℃; for 20h;
DOI:10.1002/ejoc.200400197

Reference yield:

: 652993-93-6
3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-aldehydo-D-glycero-D-ido-heptose

: 260551-08-4
3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptonic acid

Guidance literature:: With sodium chlorite; 2-methyl-but-2-ene; camphor-10-sulfonic acid; In tetrahydrofuran; isopropyl alcohol; at 20 ℃;
DOI:10.1016/S0040-4039(03)00818-9

Reference yield:

: 121123-45-3
3,4,6-tri-O-benzyl-2-acetamido-2-deoxyamino-α-D-glucopyranose

: 260551-08-4
3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / toluene; CHCl₃ / 0.5 h

2: 3.48 g / BuLi; lithium naphthalenide / tetrahydrofuran / 1 h / -78 °C

With n-butyllithium; thionyl chloride; naphthalen-1-yl-lithium; In tetrahydrofuran; chloroform; toluene; 1: Substitution / 2: Carboxylation;
DOI:10.1021/jo990766l