3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-D-ido-heptitol

Base Information

• Chemical Name: 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-D-ido-heptitol
• CAS No.: 260551-11-9
• Molecular Formula: C₃₀H₃₅NO₆
• Molecular Weight: 505.611

Synonyms:3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-D-ido-heptitol

Chemical Property of 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-D-ido-heptitol

Chemical Property:

Purity/Quality:

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Technology Process of 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-D-ido-heptitol

There total 7 articles about 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-D-ido-heptitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

S-(4-methylphenyl) 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-hepto-pyranosonothioate (768385-14-4) → 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-D-ido-heptitol (260551-11-9)

Guidance literature:

With sodium tetrahydroborate; In ethanol; dichloromethane; at 0 - 20 ℃; for 3h;

DOI:10.1002/ejoc.200400197

Reference yield: 80.0%

3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-aldehydo-D-glycero-D-ido-heptose (652993-93-6) → 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-D-ido-heptitol (260551-11-9)

Guidance literature:

With sodium tetrahydroborate; In methanol; dichloromethane; at 20 ℃; for 20h;

DOI:10.1081/CAR-120026465

Reference yield: 64.0%

3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptonic acid methyl ester (260551-09-5) → 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-1-hydroxy-D-glycero-D-ido-heptitol (260551-11-9)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; ethanol; at 0 - 20 ℃;

DOI:10.1021/jo990766l

upstream raw materials:

3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptonic acid methyl ester

3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-aldehydo-D-glycero-D-ido-heptose

S-(4-methylphenyl) 3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-hepto-pyranosonothioate

(E)-1-(2'-N-acetylamino-3',4',6'-tri-O-benzyl-2'-deoxy-α-D-glucopyranosyl)-2-propene

Downstream raw materials:

(3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-erythro-L-ido/L-gulo-heptitol-1-C-yl) dibenzyl phosphonate

(3-acetamido-2,6-anhydro-4,5,7-tri-O-benzyl-3-deoxy-D-glycero-D-ido-heptitol-1-yl) dibenzyl phosphate

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