3-butenyl formate

Base Information

• Chemical Name: 3-butenyl formate
• CAS No.: 56625-01-5
• Molecular Formula: C₅H₈O₂
• Molecular Weight: 100.117
• Mol file: 56625-01-5.mol

Synonyms:3-butenyl formate

Chemical Property of 3-butenyl formate

Chemical Property:

Purity/Quality:

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Technology Process of 3-butenyl formate

There total 4 articles about 3-butenyl formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

O-but-3-en-1-yl Se-phenyl selenocarbonate (123283-02-3) → 3-butenyl formate (56625-01-5) + 3-methyltetrahydro-2-furanone (1679-47-6)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; Heating;

DOI:10.1021/jo00043a030

Reference yield: 6.0%

cyclohexenone (930-68-7) + 2H-Pyridine-1-carboxylic acid but-3-enyl ester + dibenzoyl peroxide (94-36-0) → pyridine (110-86-1) + 3-butenyl formate (56625-01-5) + 3-butenyl benzoate (18203-32-2)

Guidance literature:

In benzene; for 48h; Product distribution; Heating;

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) → 3,4,5,6-tetrahydro-2H-pyran-2-one (542-28-9,26354-94-9) + 3-butenyl formate (56625-01-5)

Guidance literature:

With dinitrogen monoxide; In benzene; at 240 ℃; for 5h; pressure;

DOI:10.1002/adsc.200303155

upstream raw materials:

O-but-3-en-1-yl Se-phenyl selenocarbonate

cyclohexenone

dibenzoyl peroxide

3,4-dihydro-2H-pyran