10-(2-(benzylamino)ethyl)-8-chloro-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione

Base Information

Chemical Name:10-(2-(benzylamino)ethyl)-8-chloro-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione
CAS No.:1207984-80-2
Molecular Formula:C₂₀H₁₈ClN₅O₂
Molecular Weight:395.848
Hs Code.:

Synonyms:10-(2-(benzylamino)ethyl)-8-chloro-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione

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Chemical Property of 10-(2-(benzylamino)ethyl)-8-chloro-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione

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Technology Process of 10-(2-(benzylamino)ethyl)-8-chloro-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione

There total 7 articles about 10-(2-(benzylamino)ethyl)-8-chloro-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101676-75-9
(8-chloro-7-methyl-2,4-dioxo-3,4-dihydro-2H-benzo[g]pteridin-10-yl)-acetaldehyde

: 100-46-9
benzylamine

: 1207984-80-2
10-(2-(benzylamino)ethyl)-8-chloro-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: (8-chloro-7-methyl-2,4-dioxo-3,4-dihydro-2H-benzo[g]pteridin-10-yl)-acetaldehyde; benzylamine; With acetic acid; In ethanol; at 20 - 40 ℃;

With sodium cyanoborohydride; In ethanol; at 20 ℃; for 2h;

Reference yield:

: 95-74-9,827571-80-2
3-chloro-p-toluidine

: 1207984-80-2
10-(2-(benzylamino)ethyl)-8-chloro-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: Multi-step reaction with 8 steps

1.1: dmap; triethylamine / ethyl acetate / 6 h / 0 - 20 °C

2.1: nitric acid; acetic anhydride / acetic acid / 5 h / -10 - 20 °C

3.1: methanol; sodium methylate / 5 h / 20 °C

4.1: ammonium chloride / ethanol / Reflux; Inert atmosphere

5.1: sodium tetrahydroborate / ethanol / 12 h / Reflux

5.2: 0 - 20 °C

6.1: boron trioxide; acetic acid / 14 h / 20 - 70 °C / Inert atmosphere

7.1: sulfuric acid; periodic acid / water / 0 - 20 °C

7.2: pH 3.8 - 3.9

8.1: acetic acid / ethanol / 20 - 40 °C

8.2: 2 h / 20 °C

With methanol; dmap; boron trioxide; sodium tetrahydroborate; sulfuric acid; nitric acid; sodium methylate; acetic anhydride; ammonium chloride; acetic acid; periodic acid; triethylamine; In ethanol; water; acetic acid; ethyl acetate;

Reference yield:

: 1207983-26-3
(2R,3S,4S)-5-(2-amino-5-chloro-4-methylphenylamino)pentane-1,2,3,4-tetraol

: 1207984-80-2
10-(2-(benzylamino)ethyl)-8-chloro-7-methylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trioxide; acetic acid / 14 h / 20 - 70 °C / Inert atmosphere

2.1: sulfuric acid; periodic acid / water / 0 - 20 °C

2.2: pH 3.8 - 3.9

3.1: acetic acid / ethanol / 20 - 40 °C

3.2: 2 h / 20 °C

With boron trioxide; sulfuric acid; acetic acid; periodic acid; In ethanol; water;