Benzyl-2-acetamido-2,6-didesoxy-6-iod-3,4-O-isopropyliden-α-D-galactopyranosid

Base Information

Chemical Name:Benzyl-2-acetamido-2,6-didesoxy-6-iod-3,4-O-isopropyliden-α-D-galactopyranosid
CAS No.:141019-72-9
Molecular Formula:C₁₈H₂₄INO₅
Molecular Weight:461.297
Hs Code.:

Synonyms:Benzyl-2-acetamido-2,6-didesoxy-6-iod-3,4-O-isopropyliden-α-D-galactopyranosid

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Chemical Property of Benzyl-2-acetamido-2,6-didesoxy-6-iod-3,4-O-isopropyliden-α-D-galactopyranosid

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Technology Process of Benzyl-2-acetamido-2,6-didesoxy-6-iod-3,4-O-isopropyliden-α-D-galactopyranosid

There total 6 articles about Benzyl-2-acetamido-2,6-didesoxy-6-iod-3,4-O-isopropyliden-α-D-galactopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 112289-51-7
benzyl 2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside

: 141019-72-9
Benzyl-2-acetamido-2,6-didesoxy-6-iod-3,4-O-isopropyliden-α-D-galactopyranosid

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In toluene; at 60 ℃; for 2h;

Reference yield:

: 3554-93-6,347411-88-5
benzyl 2-acetamido-2-deoxy-α-D-galactopyranoside

: 141019-72-9
Benzyl-2-acetamido-2,6-didesoxy-6-iod-3,4-O-isopropyliden-α-D-galactopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / p-toluenesulfonic acid / dimethylformamide / 2 h / 60 °C

2: 64 percent / iodine, Ph₃P, imidazole / toluene / 2 h / 60 °C

With 1H-imidazole; iodine; toluene-4-sulfonic acid; triphenylphosphine; In N,N-dimethyl-formamide; toluene;

Reference yield:

: 82827-77-8
Benzyl-2-acetamido-2-desoxy-3,6-di-O-dibenzoyl-α-D-glucopyranosid

: 141019-72-9
Benzyl-2-acetamido-2,6-didesoxy-6-iod-3,4-O-isopropyliden-α-D-galactopyranosid

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / pyridine / CH₂Cl₂ / 2 h / -20 °C

2: 89 percent / NaNO₂ / dimethylformamide / 5 h / Ambient temperature

3: 1 N methanolic NaOMe / methanol / 1 h

4: 78 percent / p-toluenesulfonic acid / dimethylformamide / 2 h / 60 °C

5: 64 percent / iodine, Ph₃P, imidazole / toluene / 2 h / 60 °C

With pyridine; 1H-imidazole; iodine; sodium methylate; toluene-4-sulfonic acid; triphenylphosphine; sodium nitrite; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;