2-TRIFLUOROMETHYL-N,N-DIMETHYL-4-NITROANILINE

Base Information

• Chemical Name: 2-TRIFLUOROMETHYL-N,N-DIMETHYL-4-NITROANILINE
• CAS No.: 54672-09-2
• Molecular Formula: C9H9 F3 N2 O2
• Molecular Weight: 234.17
• Hs Code.: 2921430090
• Mol file: 54672-09-2.mol

Synonyms:Dimethyl[4-nitro-2-(trifluoromethyl)phenyl]amine;N,N-Dimethyl-4-nitro-2-trifluoromethylaniline

Chemical Property of 2-TRIFLUOROMETHYL-N,N-DIMETHYL-4-NITROANILINE

Chemical Property:

• Vapor Pressure: 0.00442mmHg at 25°C
• Boiling Point: 277.8°C at 760 mmHg
• Flash Point: 121.8°C
• PSA: 49.06000
• Density: 1.355g/cm³
• LogP: 3.20280
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

N,N-Dimethyl-4-nitro-2-(trifluoromethyl)aniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-TRIFLUOROMETHYL-N,N-DIMETHYL-4-NITROANILINE

There total 4 articles about 2-TRIFLUOROMETHYL-N,N-DIMETHYL-4-NITROANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

4-chloro-3-(trifluoromethyl)nitrobenzene (777-37-7) + N,N,N',N'-tetramethylguanidine (80-70-6) → 2-dimethylamino-5-nitrobenzotrifluoride (54672-09-2) + 2-(4-nitro-2-trifluoromethylphenyl)-1,1,3,3-tetramethylguanidine

Guidance literature:

at 20 - 100 ℃;

Reference yield:

2-Fluoro-5-nitrobenzotrifluoride (400-74-8) + dimethyl amine (124-40-3) → 2-dimethylamino-5-nitrobenzotrifluoride (54672-09-2)

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 20 - 50 ℃; for 16h;

Reference yield:

4-chloro-3-(trifluoromethyl)nitrobenzene (777-37-7) + dimethyl amine (124-40-3) → 2-dimethylamino-5-nitrobenzotrifluoride (54672-09-2)

Guidance literature:

In ethanol;

DOI:10.1055/s-1974-23461

upstream raw materials:

4-chloro-3-(trifluoromethyl)nitrobenzene

dimethyl amine

N,N,N',N'-tetramethylguanidine

2-Fluoro-5-nitrobenzotrifluoride

Downstream raw materials:

N₁,N₁-dimethyl-2-(trifluoromethyl)benzene-1,4-diamine

N,N-dimethyl-2-(trifluoromethyl)aniline

4-bromo-N,N-dimethyl-2-(trifluoromethyl)-aniline

(5-dimethylamino-2-nitro-4-trifluoromethylphenyl)acetonitrile

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