ethyl (+/-)-5-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]-2-methoxycarbonylamino-2-methylpentanoate

Base Information

Chemical Name:ethyl (+/-)-5-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]-2-methoxycarbonylamino-2-methylpentanoate
CAS No.:1006727-22-5
Molecular Formula:C₂₃H₂₅ClF₃NO₄S
Molecular Weight:503.97
Hs Code.:

Synonyms:ethyl (+/-)-5-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]-2-methoxycarbonylamino-2-methylpentanoate

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Chemical Property of ethyl (+/-)-5-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]-2-methoxycarbonylamino-2-methylpentanoate

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Technology Process of ethyl (+/-)-5-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]-2-methoxycarbonylamino-2-methylpentanoate

There total 1 articles about ethyl (+/-)-5-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]-2-methoxycarbonylamino-2-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1006727-21-4
ethyl hydrogen 2-{3-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]propyl}-2-methyl-propane dioate

: 124-41-4
sodium methylate

: 1006727-22-5
ethyl (+/-)-5-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]-2-methoxycarbonylamino-2-methylpentanoate

Guidance literature:: ethyl hydrogen 2-{3-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]propyl}-2-methyl-propane dioate; With diphenylphosphoranyl azide; triethylamine; In benzene; for 1.5h; Heating / reflux;

methanol; In benzene; at 20 ℃; for 0.833333h; Heating / reflux;

sodium methylate; In benzene; for 1.5h; Heating / reflux;

Reference yield:

: 1006727-22-5
ethyl (+/-)-5-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]-2-methoxycarbonylamino-2-methylpentanoate

: 1006727-23-6
(+/-)-5-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]-2-methoxycarbonylamino-2-methylpentan-1-ol

Guidance literature:: ethyl (+/-)-5-[2-chloro-4-(3-trifluoromethylphenylthio)phenyl]-2-methoxycarbonylamino-2-methylpentanoate; With lithium borohydride; In tetrahydrofuran; ethanol; at 0 ℃; for 1h;

With water; citric acid; In tetrahydrofuran; ethanol;