6-(2-chloroacetamido)-N-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)hexanamide

Base Information

Chemical Name:6-(2-chloroacetamido)-N-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)hexanamide
CAS No.:1509916-08-8
Molecular Formula:C₂₂H₂₄ClN₃O₃S
Molecular Weight:445.97
Hs Code.:

Synonyms:6-(2-chloroacetamido)-N-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)hexanamide

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Chemical Property of 6-(2-chloroacetamido)-N-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)hexanamide

Chemical Property:

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Technology Process of 6-(2-chloroacetamido)-N-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)hexanamide

There total 7 articles about 6-(2-chloroacetamido)-N-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 43036-17-5
2-(4-aminophenyl)-6-methoxybenzothiazole

: 140188-40-5
6-(2-chloroacetamido)hexanoyl chloride

: 1509916-08-8
6-(2-chloroacetamido)-N-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)hexanamide

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃;
DOI:10.1007/s00775-013-1055-8

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1509916-08-8
6-(2-chloroacetamido)-N-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)hexanamide

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / tetrahydrofuran / -0.16 °C

2: Lawessons reagent / chlorobenzene / Reflux

3: sodium hydroxide; potassium hexacyanoferrate(III) / Reflux

4: tin(ll) chloride / ethanol / Reflux

5: potassium carbonate / acetonitrile / 20 °C

With Lawessons reagent; potassium carbonate; triethylamine; tin(ll) chloride; sodium hydroxide; potassium hexacyanoferrate(III); In tetrahydrofuran; ethanol; chlorobenzene; acetonitrile;
DOI:10.1007/s00775-013-1055-8

Reference yield:

: 24730-11-8
N-(4-methoxyphenyl)-4-nitrobenzamide

: 1509916-08-8
6-(2-chloroacetamido)-N-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)hexanamide

Guidance literature:: Multi-step reaction with 4 steps

1: Lawessons reagent / chlorobenzene / Reflux

2: sodium hydroxide; potassium hexacyanoferrate(III) / Reflux

3: tin(ll) chloride / ethanol / Reflux

4: potassium carbonate / acetonitrile / 20 °C

With Lawessons reagent; potassium carbonate; tin(ll) chloride; sodium hydroxide; potassium hexacyanoferrate(III); In ethanol; chlorobenzene; acetonitrile;
DOI:10.1007/s00775-013-1055-8