N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-4-methoxybenzohydrazide

Base Information

Chemical Name:N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-4-methoxybenzohydrazide
CAS No.:1237587-58-4
Molecular Formula:C₂₄H₁₇Cl₃F₃N₃O₃
Molecular Weight:558.771
Hs Code.:

Synonyms:N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-4-methoxybenzohydrazide

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Chemical Property of N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-4-methoxybenzohydrazide

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Technology Process of N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-4-methoxybenzohydrazide

There total 10 articles about N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-4-methoxybenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl N'-(4-methoxybenzoyl)-N-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

: 1237587-58-4
N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-4-methoxybenzohydrazide

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 1h;

Reference yield:

: 864725-22-4
1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: 1237587-58-4
N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-4-methoxybenzohydrazide

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid / iron / ethanol / 0.83 h / 75 °C

3.1: bis(trichloromethyl) carbonate / toluene; tetrahydrofuran / 1 h / 80 °C

3.2: 16 h / 20 °C

4.1: sodium hydride / tetrahydrofuran / 0.33 h / 20 °C

4.2: 0.25 h / 20 °C

5.1: triethylamine / tetrahydrofuran / 1 h / 20 °C

6.1: trifluoroacetic acid / 1 h / 20 °C

With N-chloro-succinimide; bis(trichloromethyl) carbonate; water; sodium hydride; acetic acid; triethylamine; trifluoroacetic acid; iron; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: 66399-01-7
2-chloro-5-hydroxyiminomethylnitrobenzene

: 1237587-58-4
N′-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-4-methoxybenzohydrazide

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid / iron / ethanol / 0.83 h / 75 °C

3.1: bis(trichloromethyl) carbonate / toluene; tetrahydrofuran / 1 h / 80 °C

3.2: 16 h / 20 °C

4.1: sodium hydride / tetrahydrofuran / 0.33 h / 20 °C

4.2: 0.25 h / 20 °C

5.1: triethylamine / tetrahydrofuran / 1 h / 20 °C

6.1: trifluoroacetic acid / 1 h / 20 °C

With N-chloro-succinimide; bis(trichloromethyl) carbonate; water; sodium hydride; acetic acid; triethylamine; trifluoroacetic acid; iron; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene;