bis(2-hydroxy-3-methoxybenzylidene)succinohydrazide

Base Information

• Chemical Name: bis(2-hydroxy-3-methoxybenzylidene)succinohydrazide
• CAS No.: 346721-28-6
• Molecular Formula: C₂₀H₂₂N₄O₆
• Molecular Weight: 414.418
• Mol file: 346721-28-6.mol

Synonyms:bis(2-hydroxy-3-methoxybenzylidene)succinohydrazide

Chemical Property of bis(2-hydroxy-3-methoxybenzylidene)succinohydrazide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of bis(2-hydroxy-3-methoxybenzylidene)succinohydrazide

There total 1 articles about bis(2-hydroxy-3-methoxybenzylidene)succinohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

succinic acid dihydrazide (4146-43-4) + 3-methoxy-2-hydroxybenzaldehyde (148-53-8) → bis(2-hydroxy-3-methoxybenzylidene)succinohydrazide (346721-28-6)

Guidance literature:

In ethanol; for 4h; Reflux;

DOI:10.1016/j.jorganchem.2013.12.034

Reference yield: 89.0%

bis(2-hydroxy-3-methoxybenzylidene)succinohydrazide (346721-28-6) + diphenyltin(IV) dichloride (1135-99-5) → C44H38N4O6Sn2

Guidance literature:

With triethylamine; In ethanol; for 3.5h; Reflux;

DOI:10.1016/j.jorganchem.2013.12.034

Reference yield:

pyridine (110-86-1) + bis(2-hydroxy-3-methoxybenzylidene)succinohydrazide (346721-28-6) + titanyl perchlorate → ((C6H3(OCH3)OCHN2CO)2(CH2)2)(4-)*2TiO(2+)*2C5H5N*2C2H5OH=((C6H3(OCH3)OCHN2CO)2(CH2)2)(TiO)2(C5H5N)2(C2H5OH)2

Guidance literature:

With ethanol; In water; refluxing on a water-bath for about 6 h, pptn.; filtration, washing repeatedly with ethanol, drying in vac. over P2O5, elem. anal.;

upstream raw materials:

succinic acid dihydrazide

3-methoxy-2-hydroxybenzaldehyde