N-tert-butoxy-N-1'-phenylethyl propanamide

Base Information

Chemical Name:N-tert-butoxy-N-1'-phenylethyl propanamide
CAS No.:1208347-33-4
Molecular Formula:C₁₅H₂₃NO₂
Molecular Weight:249.353
Hs Code.:

Synonyms:N-tert-butoxy-N-1'-phenylethyl propanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-tert-butoxy-N-1'-phenylethyl propanamide

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Technology Process of N-tert-butoxy-N-1'-phenylethyl propanamide

There total 2 articles about N-tert-butoxy-N-1'-phenylethyl propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 395663-83-9
O-(tert-butyl)-N-(1-phenylethyl)hydroxylamine

: 79-03-8
propionyl chloride

: 1208347-33-4
N-tert-butoxy-N-1'-phenylethyl propanamide

Guidance literature:: With pyridine; at 0 - 20 ℃;
DOI:10.1021/jo902499s

Reference yield: 22.0%

: 1208347-20-9
N-hydroxy-N-1'-phenylethyl propanamide

: 75-65-0
tert-butyl alcohol

: 1208347-33-4
N-tert-butoxy-N-1'-phenylethyl propanamide

Guidance literature:: tert-butyl alcohol; With copper(l) chloride; diisopropyl-carbodiimide; at 20 ℃; for 120h;

N-hydroxy-N-1'-phenylethyl propanamide; In dichloromethane; at 20 ℃; for 168h;
DOI:10.1021/jo902499s

Reference yield: 70.0%

: 1208347-33-4
N-tert-butoxy-N-1'-phenylethyl propanamide

: 100-39-0
benzyl bromide

: (2RS,1'RS)-N-tert-butoxy-N-1'-phenylethyl 2-benzylpropanamide

: (2RS,1'SR)-N-(tert-butoxy)-N-1'-phenylethyl 2-benzylpropanamide

Guidance literature:: N-tert-butoxy-N-1'-phenylethyl propanamide; With potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; at -78 ℃; for 8h; Inert atmosphere;

In tetrahydrofuran; at -78 ℃; pH=7; optical yield given as %de; diastereoselective reaction; aq. phosphate buffer; Inert atmosphere;
DOI:10.1021/jo902499s