Technology Process of 2-Benzylideneheptan-1-ol
There total 9 articles about 2-Benzylideneheptan-1-ol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
formic acid; iron(II) tetrafluoroborate hexahydrate; tris(2-diphenylphosphinoethyl)phosphine;
In
tetrahydrofuran;
at 60 ℃;
for 2h;
Schlenk technique;
Inert atmosphere;
DOI:10.1016/j.jorganchem.2013.06.010
- Guidance literature:
-
With
bis(triphenylphosphine)copper(I) nitrate; hydrogen; 1,4-di(diphenylphosphino)-butane; sodium hydroxide;
In
ethanol;
at 50 ℃;
for 16h;
under 37503.8 Torr;
optical yield given as %de;
chemoselective reaction;
Autoclave;
Inert atmosphere;
DOI:10.1055/s-0028-1216726
- Guidance literature:
-
With
chlorine[2-(4,5-dihydro-1H-imidazol-2-yl)-6-methoxypyridine](pentamethylcyclopentadienyl)iridium(III) chloride; sodium formate;
In
water;
at 80 ℃;
for 0.5h;
chemoselective reaction;
Schlenk technique;
DOI:10.1021/acs.organomet.9b00353
