[2-(4-azido-2-hydroxy-benzoylamino)-ethyl]-carbamicacid tert-butyl ester

Base Information

Chemical Name:[2-(4-azido-2-hydroxy-benzoylamino)-ethyl]-carbamicacid tert-butyl ester
CAS No.:1293988-98-3
Molecular Formula:C₁₄H₁₉N₅O₄
Molecular Weight:321.336
Hs Code.:

Synonyms:[2-(4-azido-2-hydroxy-benzoylamino)-ethyl]-carbamicacid tert-butyl ester

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Chemical Property of [2-(4-azido-2-hydroxy-benzoylamino)-ethyl]-carbamicacid tert-butyl ester

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Technology Process of [2-(4-azido-2-hydroxy-benzoylamino)-ethyl]-carbamicacid tert-butyl ester

There total 2 articles about [2-(4-azido-2-hydroxy-benzoylamino)-ethyl]-carbamicacid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 57260-73-8
N-BOC-1,2-diaminoethane

: 66761-27-1
4-carboxy-3-hydroxyphenyl azide

: 1892-57-5,754131-18-5
N-(3-dimethylaminopropyl)-N-ethylcarbodiimide

: 1293988-98-3
[2-(4-azido-2-hydroxy-benzoylamino)-ethyl]-carbamicacid tert-butyl ester

Guidance literature:: 4-carboxy-3-hydroxyphenyl azide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; With benzotriazol-1-ol; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

N-BOC-1,2-diaminoethane; In N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1002/bkcs.10453