β-allyl (2S)-N-(fluoren-9-ylmethoxycarbonyl)phenylalanyl-β-alanyl-[α-methyl (2R)-glutamyl]-γ-(2S)-prolyl-[(2R)-aspartate] diester

Base Information

Chemical Name:β-allyl (2S)-N-(fluoren-9-ylmethoxycarbonyl)phenylalanyl-β-alanyl-[α-methyl (2R)-glutamyl]-γ-(2S)-prolyl-[(2R)-aspartate] diester
CAS No.:195301-96-3
Molecular Formula:C₄₅H₅₁N₅O₁₂
Molecular Weight:853.926
Hs Code.:

Synonyms:β-allyl (2S)-N-(fluoren-9-ylmethoxycarbonyl)phenylalanyl-β-alanyl-[α-methyl (2R)-glutamyl]-γ-(2S)-prolyl-[(2R)-aspartate] diester

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Chemical Property of β-allyl (2S)-N-(fluoren-9-ylmethoxycarbonyl)phenylalanyl-β-alanyl-[α-methyl (2R)-glutamyl]-γ-(2S)-prolyl-[(2R)-aspartate] diester

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Technology Process of β-allyl (2S)-N-(fluoren-9-ylmethoxycarbonyl)phenylalanyl-β-alanyl-[α-methyl (2R)-glutamyl]-γ-(2S)-prolyl-[(2R)-aspartate] diester

There total 3 articles about β-allyl (2S)-N-(fluoren-9-ylmethoxycarbonyl)phenylalanyl-β-alanyl-[α-methyl (2R)-glutamyl]-γ-(2S)-prolyl-[(2R)-aspartate] diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 368443-68-9
α-methyl γ-allyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)glutamate

: 195301-96-3
β-allyl (2S)-N-(fluoren-9-ylmethoxycarbonyl)phenylalanyl-β-alanyl-[α-methyl (2R)-glutamyl]-γ-(2S)-prolyl-[(2R)-aspartate] diester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / PhSiH₃ / (Ph₃P)4Pd⁽⁰⁾ / CH₂Cl₂ / 2 h / 20 °C

With phenylsilane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane;
DOI:10.1039/b100401h

Reference yield:

: 204251-33-2
γ-allyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)glutamate

: 195301-96-3
β-allyl (2S)-N-(fluoren-9-ylmethoxycarbonyl)phenylalanyl-β-alanyl-[α-methyl (2R)-glutamyl]-γ-(2S)-prolyl-[(2R)-aspartate] diester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / diethyl ether / 1 h / 0 °C

2: 81 percent / PhSiH₃ / (Ph₃P)4Pd⁽⁰⁾ / CH₂Cl₂ / 2 h / 20 °C

With phenylsilane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; dichloromethane;
DOI:10.1039/b100401h