2-phenylpyrimidine-4,6-dicarboxaldehyde bis{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]2-phenylpyrimidin-4-yl}hydrazone}

Base Information

• Chemical Name: 2-phenylpyrimidine-4,6-dicarboxaldehyde bis{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]2-phenylpyrimidin-4-yl}hydrazone}
• CAS No.: 618428-70-9
• Molecular Formula: C₄₈H₄₂N₁₆
• Molecular Weight: 842.969
• Mol file: 618428-70-9.mol

Synonyms:2-phenylpyrimidine-4,6-dicarboxaldehyde bis{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]2-phenylpyrimidin-4-yl}hydrazone}

Chemical Property of 2-phenylpyrimidine-4,6-dicarboxaldehyde bis{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]2-phenylpyrimidin-4-yl}hydrazone}

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-phenylpyrimidine-4,6-dicarboxaldehyde bis{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]2-phenylpyrimidin-4-yl}hydrazone}

There total 4 articles about 2-phenylpyrimidine-4,6-dicarboxaldehyde bis{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]2-phenylpyrimidin-4-yl}hydrazone} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

ethanol (64-17-5) + 2-phenyl-4,6-pyrimidinedicarboxaldehyde (80109-86-0) + pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-phenylpyrimidin-4-yl]hydrazone (618428-59-4) → 2-phenylpyrimidine-4,6-dicarboxaldehyde mono{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]-2-phenylpyrimidin-4-yl}hydrazone} + 2-phenylpyrimidine-4,6-dicarboxaldehyde bis{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]2-phenylpyrimidin-4-yl}hydrazone} (618428-70-9)

Guidance literature:

In chloroform; at 20 ℃; for 2h;

DOI:10.1002/hlca.200390137

Reference yield:

pyridine-2-carbaldehyde (1121-60-4) → 2-phenylpyrimidine-4,6-dicarboxaldehyde bis{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]2-phenylpyrimidin-4-yl}hydrazone} (618428-70-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / ethanol / 3 h / 20 °C

2: 8 percent / CHCl₃ / 2 h / 20 °C

In ethanol; chloroform;

DOI:10.1002/hlca.200390137

Reference yield:

fenclorim (3740-92-9) → 2-phenylpyrimidine-4,6-dicarboxaldehyde bis{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]2-phenylpyrimidin-4-yl}hydrazone} (618428-70-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 70 percent / ethanol / 48 h / Heating

2: 80 percent / ethanol / 3 h / 20 °C

3: 8 percent / CHCl₃ / 2 h / 20 °C

In ethanol; chloroform;

DOI:10.1002/hlca.200390137

upstream raw materials:

ethanol

2-phenyl-4,6-pyrimidinedicarboxaldehyde

pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-phenylpyrimidin-4-yl]hydrazone

pyridine-2-carbaldehyde

Downstream raw materials:

pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidin-4-yl]hydrazone

pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-phenylpyrimidin-4-yl]hydrazone

4,6-bis{[N-methyl-N'-(pyridin-2-yl)methylidene]hydrazino}-2-phenylpyrimidine