4,6-bis{[N-methyl-N'-(pyridin-2-yl)methylidene]hydrazino}-2-phenylpyrimidine

Base Information

Chemical Name:4,6-bis{[N-methyl-N'-(pyridin-2-yl)methylidene]hydrazino}-2-phenylpyrimidine
CAS No.:618428-41-4
Molecular Formula:C₂₄H₂₂N₈
Molecular Weight:422.492
Hs Code.:

Synonyms:4,6-bis{[N-methyl-N'-(pyridin-2-yl)methylidene]hydrazino}-2-phenylpyrimidine

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Chemical Property of 4,6-bis{[N-methyl-N'-(pyridin-2-yl)methylidene]hydrazino}-2-phenylpyrimidine

Chemical Property:

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Technology Process of 4,6-bis{[N-methyl-N'-(pyridin-2-yl)methylidene]hydrazino}-2-phenylpyrimidine

There total 2 articles about 4,6-bis{[N-methyl-N'-(pyridin-2-yl)methylidene]hydrazino}-2-phenylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 618428-27-6
4,6-bis(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidine

: 618428-70-9
2-phenylpyrimidine-4,6-dicarboxaldehyde bis{methyl{6-[1-methyl-2-(pyridin-2-ylmethylene)hydrazino]2-phenylpyrimidin-4-yl}hydrazone}

: 798569-44-5
pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidin-4-yl]hydrazone

: 618428-59-4
pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-phenylpyrimidin-4-yl]hydrazone

: 618428-41-4
4,6-bis{[N-methyl-N'-(pyridin-2-yl)methylidene]hydrazino}-2-phenylpyrimidine

: pyridine 2-carboxaldehyde [2-(3,4,5-trimethoxyphenyl)pyrimidine-4,6-diyl]bis(methylhydrazone)

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In chloroform; at 60 ℃; for 48h; Further byproducts given. Title compound not separated from byproducts;
DOI:10.1021/ja0666452

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 618428-22-1
4,6-bis(1-methylhydrazinyl)-2-phenyl-1-pyrimidine

: 618428-41-4
4,6-bis{[N-methyl-N'-(pyridin-2-yl)methylidene]hydrazino}-2-phenylpyrimidine

Guidance literature:: In ethanol; for 3h; Heating;
DOI:10.1002/ejic.200500963

Reference yield:

: 618428-27-6
4,6-bis(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidine

: 618428-41-4
4,6-bis{[N-methyl-N'-(pyridin-2-yl)methylidene]hydrazino}-2-phenylpyrimidine

: 798569-44-5
pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidin-4-yl]hydrazone

: 618428-22-1
4,6-bis(1-methylhydrazinyl)-2-phenyl-1-pyrimidine

: 618428-59-4
pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-phenylpyrimidin-4-yl]hydrazone

: pyridine 2-carboxaldehyde [2-(3,4,5-trimethoxyphenyl)pyrimidine-4,6-diyl]bis(methylhydrazone)

Guidance literature:: zinc tetrafluoroborate; In chloroform; at 60 ℃; Further Variations:; Catalysts; Product distribution;
DOI:10.1002/anie.200460343