pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidin-4-yl]hydrazone

Base Information

Chemical Name:pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidin-4-yl]hydrazone
CAS No.:798569-44-5
Molecular Formula:C₂₁H₂₅N₇O₃
Molecular Weight:423.475
Hs Code.:

Synonyms:pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidin-4-yl]hydrazone

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Chemical Property of pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidin-4-yl]hydrazone

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Technology Process of pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidin-4-yl]hydrazone

There total 7 articles about pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidin-4-yl]hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1121-60-4
pyridine-2-carbaldehyde

: 618428-27-6
4,6-bis(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidine

: 798569-44-5
pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidin-4-yl]hydrazone

Guidance literature:: In ethanol; chloroform; at 20 ℃; for 24h;
DOI:10.1021/ja0666452

Reference yield:

: C₆₉H₆₃N₁₉O₆

: 618428-27-6
4,6-bis(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidine

: 798569-44-5
pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidin-4-yl]hydrazone

: C₆₃H₆₀N₁₈O₆

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In chloroform-d1; at 60 ℃; for 1.66667h; Title compound not separated from byproducts;
DOI:10.1021/ja0666452

Reference yield:

: 1-(6-(methoxymethyl)-2-phenylpyrimidin-4-yl)-1-methyl-2-(pyridin-2-ylmethylene)hydrazine

: 618428-27-6
4,6-bis(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidine

: 798569-44-5
pyridine-2-carboxaldehyde methyl[6-(1-methylhydrazino)-2-(3,4,5-trimethoxyphenyl)pyrimidin-4-yl]hydrazone

: 922726-19-0
1-(6-(methoxymethyl)-2-phenylpyrimidin-4-yl)-1-methylhydrazine

: pyridine 2-carboxaldehyde [2-(3,4,5-trimethoxyphenyl)pyrimidine-4,6-diyl]bis(methylhydrazone)

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In various solvent(s); at 140 ℃; for 0.0666667h; Title compound not separated from byproducts; microwave heating;
DOI:10.1021/ja0666452