[Rh(H)(C₁₃H₈N)(P(C₆H₅)3)2(OC(CH₃)2)]⁽¹⁺⁾*PF₆^(1-)=[Rh(H)(C₁₃H₈N)(P(C₆H₅)3)2(OC(CH₃)2)]PF₆

Base Information

• Chemical Name: [Rh(H)(C₁₃H₈N)(P(C₆H₅)3)2(OC(CH₃)2)]⁽¹⁺⁾*PF₆^(1-)=[Rh(H)(C₁₃H₈N)(P(C₆H₅)3)2(OC(CH₃)2)]PF₆
• CAS No.: 1092577-01-9
• Molecular Formula: C₅₂H₄₅NOP₂Rh*F₆P
• Molecular Weight: 1009.75

Synonyms:[Rh(H)(C₁₃H₈N)(P(C₆H₅)3)2(OC(CH₃)2)]⁽¹⁺⁾*PF₆^(1-)=[Rh(H)(C₁₃H₈N)(P(C₆H₅)3)2(OC(CH₃)2)]PF₆

Chemical Property of [Rh(H)(C₁₃H₈N)(P(C₆H₅)3)2(OC(CH₃)2)]⁽¹⁺⁾*PF₆^(1-)=[Rh(H)(C₁₃H₈N)(P(C₆H₅)3)2(OC(CH₃)2)]PF₆

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Technology Process of [Rh(H)(C₁₃H₈N)(P(C₆H₅)3)2(OC(CH₃)2)]⁽¹⁺⁾*PF₆^(1-)=[Rh(H)(C₁₃H₈N)(P(C₆H₅)3)2(OC(CH₃)2)]PF₆

There total 1 articles about [Rh(H)(C₁₃H₈N)(P(C₆H₅)3)2(OC(CH₃)2)]⁽¹⁺⁾*PF₆^(1-)=[Rh(H)(C₁₃H₈N)(P(C₆H₅)3)2(OC(CH₃)2)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

7,8-benzoquinoline (230-27-3) + [Rh(I)(norbornadiene)(PPh3)2]PF6 (32799-32-9) + hydrogen (1333-74-0) + acetone (67-64-1) → [Rh(H)(C13H8N)(P(C6H5)3)2(OC(CH3)2)](1+)*PF6(1-)=[Rh(H)(C13H8N)(P(C6H5)3)2(OC(CH3)2)]PF6 (1092577-01-9)

Guidance literature:

With tert-butylethylene; In acetone; (Schlenk); bubbling H2 through a suspn. of Rh complex in acetone for 15 min at 0°C, addn. of tert-butylethylene and ligand, reflux for 5 h; concentration under reduced pressure, washing with OEt2, elem. anal.;

DOI:10.1021/ic801878e

Reference yield: 73.0%

[Rh(H)(C13H8N)(P(C6H5)3)2(OC(CH3)2)](1+)*PF6(1-)=[Rh(H)(C13H8N)(P(C6H5)3)2(OC(CH3)2)]PF6 (1092577-01-9) + iodine (7553-56-2,12190-71-5,8031-47-8) → Rh(C13H8N)I2(P(C6H5)3)2 (1103534-60-6)

Guidance literature:

In tetrahydrofuran; byproducts: HPF6; (Schlenk); I2 addn. to suspn. of Rh complex in THF, stirring for 4 h at 0°C; filtration, washing ppt. with OEt2, diffusion of OEt2 into CH2Cl2 soln.;elem. anal.;

DOI:10.1021/ic801878e

upstream raw materials:

7,8-benzoquinoline

[Rh(I)(norbornadiene)(PPh₃)2]PF₆

hydrogen

acetone

Downstream raw materials:

Rh(C₁₃H₈N)I₂(P(C₆H₅)3)2

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