(4-Methoxybenzylidene)(4-chlorophenyl)methylamine

Base Information

• Chemical Name: (4-Methoxybenzylidene)(4-chlorophenyl)methylamine
• CAS No.: 72954-74-6
• Molecular Formula: C₁₅H₁₄ClNO
• Molecular Weight: 259.735
• Mol file: 72954-74-6.mol

Synonyms:(4-Methoxybenzylidene)(4-chlorophenyl)methylamine

Chemical Property of (4-Methoxybenzylidene)(4-chlorophenyl)methylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4-Methoxybenzylidene)(4-chlorophenyl)methylamine

There total 4 articles about (4-Methoxybenzylidene)(4-chlorophenyl)methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chlorobenzylamine (104-86-9) + 4-Methoxybenzyl alcohol (105-13-5) → (4-Methoxybenzylidene)(4-chlorophenyl)methylamine (72954-74-6)

Guidance literature:

With C₂₈H₂₈Cl₂Cu₂N₄; oxygen; potassium hydroxide; In toluene; at 60 ℃; for 8h;

DOI:10.1016/j.jorganchem.2017.05.009

Reference yield:

4-methoxy-benzaldehyde (123-11-5) + 4-chlorobenzylamine (104-86-9) → (4-Methoxybenzylidene)(4-chlorophenyl)methylamine (72954-74-6)

Guidance literature:

With orthoformic acid triethyl ester; In tetrahydrofuran;

DOI:10.1021/co2001873

Reference yield:

4-chlorobenzylamine (104-86-9) + 4-methoxybenzonitrile (874-90-8) → (4-Methoxybenzylidene)(4-chlorophenyl)methylamine (72954-74-6)

Guidance literature:

With C₂₂H₄₀BrFeNOP₂; potassium tert-butylate; hydrogen; In benzene; at 60 ℃; for 12h; under 15001.5 Torr; Inert atmosphere; Glovebox; Schlenk technique; Autoclave;

DOI:10.1002/anie.201608537

upstream raw materials:

4-methoxy-benzaldehyde

4-chlorobenzylamine

4-methoxybenzonitrile

4-Methoxybenzyl alcohol