4--buttersaeure-methylester

Base Information

• Chemical Name: 4--buttersaeure-methylester
• CAS No.: 92196-82-2
• Molecular Formula: C₁₃H₁₉NO₂
• Molecular Weight: 221.299

Synonyms:4--buttersaeure-methylester

Chemical Property of 4--buttersaeure-methylester

Chemical Property:

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Technology Process of 4--buttersaeure-methylester

There total 4 articles about 4--buttersaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

methanol (67-56-1) + 4-(N-benzyl-N-methylamino)-1-diazobutan-2-one → 4--buttersaeure-methylester (92196-82-2)

Guidance literature:

With [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold(I); at 20 ℃; for 6h;

DOI:10.1021/ja208860x

Reference yield:

Methyl 4-bromobutyrate (4897-84-1) + benzyl-methyl-amine (103-67-3) → 4--buttersaeure-methylester (92196-82-2)

Guidance literature:

With potassium carbonate; In acetonitrile; at 55 ℃; for 8h;

Reference yield:

methyl 4-iodobutanoate (14273-85-9) + benzyl-methyl-amine (103-67-3) → 4--buttersaeure-methylester (92196-82-2)

Guidance literature:

In toluene; Heating;

DOI:10.1021/ja01474a024

upstream raw materials:

methyl 4-iodobutanoate

benzyl-methyl-amine

methanol

Methyl 4-bromobutyrate

Downstream raw materials:

4-[benzyl(methyl)amino]butanoic acid

5-(benzyl-methyl-amino)-pentan-2-one

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