4-methoxy-3-phenylisoquinoline

Base Information

Chemical Name:4-methoxy-3-phenylisoquinoline
CAS No.:57703-37-4
Molecular Formula:C₁₆H₁₃NO
Molecular Weight:235.285
Hs Code.:

Synonyms:4-methoxy-3-phenylisoquinoline

Suppliers and Price of 4-methoxy-3-phenylisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxy-3-phenylisoquinoline

Chemical Property:

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Technology Process of 4-methoxy-3-phenylisoquinoline

There total 9 articles about 4-methoxy-3-phenylisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1394823-26-7
C₁₈H₁₈O₄

: 57703-37-4
4-methoxy-3-phenylisoquinoline

Guidance literature:: With ammonium chloride; In ethanol; water; at 90 ℃; for 24h;
DOI:10.1073/pnas.1206532109

Reference yield: 80.0%

: 4079-52-1
methoxymethyl phenyl ketone

: 1314031-74-7
(E)-2-bromobenzaldehyde O-methyl oxime

: 57703-37-4
4-methoxy-3-phenylisoquinoline

Guidance literature:: methoxymethyl phenyl ketone; (E)-2-bromobenzaldehyde O-methyl oxime; With bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); caesium carbonate; In tetrahydrofuran; at 70 ℃; for 18h; Inert atmosphere; Sealed tube;

With ammonium hydroxide; ammonium chloride; In ethanol; water; at 110 ℃; for 24h; pH=Ca. 9;
DOI:10.1039/c5ob02320c

Reference yield: 15.0%

: 67-56-1
methanol

: 37993-76-3
3-phenylisoquinoline

: 57703-37-4
4-methoxy-3-phenylisoquinoline

: (3-phenylisoquinolin-1-yl)methanol

: (4-methoxy-3-phenylisoquinolin-1-yl)-methanol

Guidance literature:: With [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; trifluoroacetic acid; dibenzoyl peroxide; for 8h; Inert atmosphere; Autoclave; Glovebox; UV-irradiation;
DOI:10.1021/acs.joc.6b00811