1-(5-O-benzoyl-3-deoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)thymine

Base Information

Chemical Name:1-(5-O-benzoyl-3-deoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)thymine
CAS No.:133272-14-7
Molecular Formula:C₂₂H₂₉N₂O₉P
Molecular Weight:496.454
Hs Code.:

Synonyms:1-(5-O-benzoyl-3-deoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)thymine

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Chemical Property of 1-(5-O-benzoyl-3-deoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)thymine

Chemical Property:

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Technology Process of 1-(5-O-benzoyl-3-deoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)thymine

There total 2 articles about 1-(5-O-benzoyl-3-deoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 91592-49-3
1-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)thymine

: 133272-15-8
Benzoic acid (2S,3S,4R,5R)-3-(ethoxy-hydroxy-phosphorylmethyl)-4-hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl ester

: 133272-14-7
1-(5-O-benzoyl-3-deoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)thymine

Guidance literature:: With pyridine; hydroxylamine acetate; for 26h; Ambient temperature;

Reference yield:

: 65-71-4,80289-22-1
2,4-dihydroxy-5-methylpyrimidine

: 133272-14-7
1-(5-O-benzoyl-3-deoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)thymine

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / 1.) hexamethyldisilazane (HDMS), chlorotrimethylsilane (CTS), pyridine, 2.) potassium perfluorobutanesulfonate (KPBS), CTS / 1.) reflux, 2.) MeCN, dichloroethane, reflux, 4 h

2: 63 percent / hydroxylammonium acetate, pyridine / 26 h / Ambient temperature

With pyridine; chloro-trimethyl-silane; hydroxylamine acetate; potassium nonaflate; 1,1,1,3,3,3-hexamethyl-disilazane;