(R)-6-bromo-1-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)-1H-benzo[d][1,2,3]triazole

Base Information

Chemical Name:(R)-6-bromo-1-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)-1H-benzo[d][1,2,3]triazole
CAS No.:1442445-65-9
Molecular Formula:C₁₅H₁₀BrClF₃N₃
Molecular Weight:404.617
Hs Code.:

Synonyms:(R)-6-bromo-1-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)-1H-benzo[d][1,2,3]triazole

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Chemical Property of (R)-6-bromo-1-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)-1H-benzo[d][1,2,3]triazole

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Technology Process of (R)-6-bromo-1-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)-1H-benzo[d][1,2,3]triazole

There total 6 articles about (R)-6-bromo-1-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)-1H-benzo[d][1,2,3]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1442445-64-8
(R)-5-bromo-N-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)benzene-1,2-diamine

: 64-19-7,77671-22-8
acetic acid

: 1442445-65-9
(R)-6-bromo-1-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)-1H-benzo[d][1,2,3]triazole

Guidance literature:: With sodium nitrite; at 20 ℃; for 18h;

Reference yield:

: 1442445-19-3
(S)-N-(4-chloro-2-(trifluoromethyl)benzylidene)-2-methylpropane-2-sulfinamide

: 1442445-65-9
(R)-6-bromo-1-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)-1H-benzo[d][1,2,3]triazole

Guidance literature:: Multi-step reaction with 5 steps

1: dichloromethane; diethyl ether / 18 h / -48 °C

2: hydrogenchloride / methanol; 1,4-dioxane / 0.5 h / 20 °C

3: potassium carbonate / dimethyl sulfoxide / 1 h / 120 °C

4: hydrogenchloride; iron / ethanol; water / 0.75 h / 90 °C

5: sodium nitrite / 18 h / 20 °C

With hydrogenchloride; iron; potassium carbonate; sodium nitrite; In 1,4-dioxane; methanol; diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: 1442445-20-6
(S)-N-((R)-1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)-2-methylpropane-2-sulfinamide

: 1442445-65-9
(R)-6-bromo-1-(1-(4-chloro-2-(trifluoromethyl)phenyl)ethyl)-1H-benzo[d][1,2,3]triazole

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / methanol; 1,4-dioxane / 0.5 h / 20 °C

2: potassium carbonate / dimethyl sulfoxide / 1 h / 120 °C

3: hydrogenchloride; iron / ethanol; water / 0.75 h / 90 °C

4: sodium nitrite / 18 h / 20 °C

With hydrogenchloride; iron; potassium carbonate; sodium nitrite; In 1,4-dioxane; methanol; ethanol; water; dimethyl sulfoxide;