Technology Process of methyl 2-iodo-3,4-diisobutoxybenzoate
There total 6 articles about methyl 2-iodo-3,4-diisobutoxybenzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-iodo-3,4-diisobutoxybenzoic acid;
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.333333h;
Inert atmosphere;
methyl iodide;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ol401197n
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium permanganate / water; acetone / 36 h / 20 °C / Inert atmosphere
2.1: potassium carbonate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere
2.2: 2 h / 0 - 20 °C / Inert atmosphere
With
potassium permanganate; potassium carbonate;
In
water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ol401197n
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine; aluminum (III) chloride / dichloromethane / 20.08 h / 0 °C / Inert atmosphere; Reflux
2.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
2.2: 72 h / 50 °C / Inert atmosphere
3.1: potassium permanganate / water; acetone / 36 h / 20 °C / Inert atmosphere
4.1: potassium carbonate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere
4.2: 2 h / 0 - 20 °C / Inert atmosphere
With
pyridine; aluminum (III) chloride; potassium permanganate; potassium carbonate;
In
dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ol401197n
